3-(1-(4-bromophenyl)-3-phenylprop-2-ynyl)-9-methyl-6-(1-p-tolylhept-2-ynyl)-9H-carbazole

Base Information

Chemical Name:3-(1-(4-bromophenyl)-3-phenylprop-2-ynyl)-9-methyl-6-(1-p-tolylhept-2-ynyl)-9H-carbazole
CAS No.:1421675-19-5
Molecular Formula:C₄₂H₃₆BrN
Molecular Weight:634.659
Hs Code.:

Synonyms:3-(1-(4-bromophenyl)-3-phenylprop-2-ynyl)-9-methyl-6-(1-p-tolylhept-2-ynyl)-9H-carbazole

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Chemical Property of 3-(1-(4-bromophenyl)-3-phenylprop-2-ynyl)-9-methyl-6-(1-p-tolylhept-2-ynyl)-9H-carbazole

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Technology Process of 3-(1-(4-bromophenyl)-3-phenylprop-2-ynyl)-9-methyl-6-(1-p-tolylhept-2-ynyl)-9H-carbazole

There total 4 articles about 3-(1-(4-bromophenyl)-3-phenylprop-2-ynyl)-9-methyl-6-(1-p-tolylhept-2-ynyl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 191403-25-5
1-(4-fluorophenyl)hept-2-yn-1-ol

: 1484-12-4
N-methylcarbazole

: 142739-40-0
1-(4-bromo-phenyl)-3-phenyl-prop-2-yn-1-ol

: 1421675-09-3
3,6-bis(1-(4-bromophenyl)-3-phenylprop-2-ynyl)-9-methyl-9H-carbazole

: 1421675-14-0
9-methyl-3,6-bis(1-p-tolylhept-2-ynyl)-9H-carbazole

: 1421675-19-5
3-(1-(4-bromophenyl)-3-phenylprop-2-ynyl)-9-methyl-6-(1-p-tolylhept-2-ynyl)-9H-carbazole

Guidance literature:: N-methylcarbazole; 1-(4-bromo-phenyl)-3-phenyl-prop-2-yn-1-ol; With bismuth (III) nitrate pentahydrate; at 20 - 70 ℃; Ionic liquid; Inert atmosphere; Schlenk technique;

1-(p-fluorophenyl)-2-heptyn-1-ol; With bismuth (III) nitrate pentahydrate; at 20 - 70 ℃; Inert atmosphere; Ionic liquid; Schlenk technique;
DOI:10.1016/j.tetlet.2012.12.023

Reference yield:

: 536-74-3
phenylacetylene

: 1421675-19-5
3-(1-(4-bromophenyl)-3-phenylprop-2-ynyl)-9-methyl-6-(1-p-tolylhept-2-ynyl)-9H-carbazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; zinc(II) chloride / toluene / 1 h / 20 °C

1.2: 12 h

2.1: bismuth (III) nitrate pentahydrate / 20 - 70 °C / Ionic liquid; Inert atmosphere; Schlenk technique

2.2: 20 - 70 °C / Inert atmosphere; Ionic liquid; Schlenk technique

With bismuth (III) nitrate pentahydrate; triethylamine; zinc(II) chloride; In toluene;
DOI:10.1016/j.tetlet.2012.12.023

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1421675-14-0
9-methyl-3,6-bis(1-p-tolylhept-2-ynyl)-9H-carbazole

: 1421675-19-5
3-(1-(4-bromophenyl)-3-phenylprop-2-ynyl)-9-methyl-6-(1-p-tolylhept-2-ynyl)-9H-carbazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; zinc(II) chloride / toluene / 1 h / 20 °C

1.2: 12 h

2.1: bismuth (III) nitrate pentahydrate / 20 - 70 °C / Ionic liquid; Inert atmosphere; Schlenk technique

2.2: 20 - 70 °C / Inert atmosphere; Ionic liquid; Schlenk technique

With bismuth (III) nitrate pentahydrate; triethylamine; zinc(II) chloride; In toluene;
DOI:10.1016/j.tetlet.2012.12.023