N',N''-dioctadecyl-N-[(benzyloxy)carbonyl]-L-glutamamide

Base Information

Chemical Name:N',N''-dioctadecyl-N-[(benzyloxy)carbonyl]-L-glutamamide
CAS No.:128701-80-4
Molecular Formula:C₄₉H₈₉N₃O₄
Molecular Weight:784.263
Hs Code.:

Synonyms:N',N''-dioctadecyl-N-[(benzyloxy)carbonyl]-L-glutamamide

Suppliers and Price of N',N''-dioctadecyl-N-[(benzyloxy)carbonyl]-L-glutamamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N',N''-dioctadecyl-N-[(benzyloxy)carbonyl]-L-glutamamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of N',N''-dioctadecyl-N-[(benzyloxy)carbonyl]-L-glutamamide

There total 2 articles about N',N''-dioctadecyl-N-[(benzyloxy)carbonyl]-L-glutamamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1155-62-0
N-benzyloxycarbonyl-L-glutamic acid

: 124-30-1
1-aminooctadecane

: 128701-80-4
N',N''-dioctadecyl-N-[(benzyloxy)carbonyl]-L-glutamamide

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/ac050851v

Reference yield:

: 56-86-0,21675-62-7,23009-64-5,25104-13-6,84960-48-5,25513-46-6
L-glutamic acid

: 501-53-1,94274-21-2
benzyl chloroformate

: 128701-80-4
N',N''-dioctadecyl-N-[(benzyloxy)carbonyl]-L-glutamamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water / 0 - 20 °C / pH 12

2: diethyl cyanophosphonate; triethylamine / tetrahydrofuran / 0 °C

With diethyl cyanophosphonate; triethylamine; sodium hydroxide; In tetrahydrofuran; water;
DOI:10.1039/c1cc13397g

Reference yield:

: 128701-80-4
N',N''-dioctadecyl-N-[(benzyloxy)carbonyl]-L-glutamamide

: 148417-40-7
N',N''-dioctadecyl-N^α-carbobenzoyl-α-alanyl-L-glutamide

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / tetrahydrofuran; ethanol / 60 °C

2: diethyl cyanophosphonate; triethylamine / tetrahydrofuran / 1 h / 0 °C

With diethyl cyanophosphonate; palladium on activated charcoal; hydrogen; triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1039/c1cc13397g