10b-Methyl-2,3-diphenyl-1-oxo-1,5,6,10b-tetrahydropyrrolo<2.1-a>isochinolin

Base Information

Chemical Name:10b-Methyl-2,3-diphenyl-1-oxo-1,5,6,10b-tetrahydropyrrolo<2.1-a>isochinolin
CAS No.:71611-89-7
Molecular Formula:C₂₅H₂₁NO
Molecular Weight:351.448
Hs Code.:

Synonyms:10b-Methyl-2,3-diphenyl-1-oxo-1,5,6,10b-tetrahydropyrrolo<2.1-a>isochinolin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10b-Methyl-2,3-diphenyl-1-oxo-1,5,6,10b-tetrahydropyrrolo<2.1-a>isochinolin

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Technology Process of 10b-Methyl-2,3-diphenyl-1-oxo-1,5,6,10b-tetrahydropyrrolo<2.1-a>isochinolin

There total 5 articles about 10b-Methyl-2,3-diphenyl-1-oxo-1,5,6,10b-tetrahydropyrrolo<2.1-a>isochinolin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 2412-58-0
1-methyl-3,4,dihydroisoquinoline

: 886-38-4
diphenylcyclopropenone

: 71611-89-7
10b-Methyl-2,3-diphenyl-1-oxo-1,5,6,10b-tetrahydropyrrolo<2.1-a>isochinolin

Guidance literature:: In ethanol; for 1h; Heating;
DOI:10.1055/s-1986-31820

Reference yield: 78.0%

: 71611-94-4
10b-Methyl-2,3-diphenyl-1-thioxo-1,5,6,10b-tetrahydropyrrolo<2.1-a>isochinolin

: 71611-89-7
10b-Methyl-2,3-diphenyl-1-oxo-1,5,6,10b-tetrahydropyrrolo<2.1-a>isochinolin

Guidance literature:: With mesitylenecarbonitrile oxide; In acetonitrile; Heating;
DOI:10.1055/s-1986-31820

Reference yield:

: 2412-58-0
1-methyl-3,4,dihydroisoquinoline

: 71611-89-7
10b-Methyl-2,3-diphenyl-1-oxo-1,5,6,10b-tetrahydropyrrolo<2.1-a>isochinolin

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / 1,2-dimethoxy-ethane / 15 h / 20 °C

2: 78 percent / mesitonitriloxide / acetonitrile / Heating

With mesitylenecarbonitrile oxide; In 1,2-dimethoxyethane; acetonitrile;
DOI:10.1055/s-1986-31820