1-[(p-methylphenyl)thio]ethyl butyl ether

Base Information

• Chemical Name: 1-[(p-methylphenyl)thio]ethyl butyl ether
• CAS No.: 1609649-40-2
• Molecular Formula: C₁₃H₂₀OS
• Molecular Weight: 224.367
• Mol file: 1609649-40-2.mol

Synonyms:1-[(p-methylphenyl)thio]ethyl butyl ether

Chemical Property of 1-[(p-methylphenyl)thio]ethyl butyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-[(p-methylphenyl)thio]ethyl butyl ether

There total 2 articles about 1-[(p-methylphenyl)thio]ethyl butyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

-butyl vinyl ether (111-34-2,92680-80-3) + para-thiocresol (106-45-6) → 1-[(p-methylphenyl)thio]ethyl butyl ether (1609649-40-2)

Guidance literature:

With oxygen; copper diacetate; In dichloromethane; at 50 ℃; for 3h; Reagent/catalyst; Time; Solvent; Sealed tube;

DOI:10.1016/j.tet.2016.05.050

Reference yield:

-butyl vinyl ether (111-34-2,92680-80-3) + para-thiocresol (106-45-6) → 1,1-bis<(4-methylphenyl)thio>ethane (33451-45-5) + 1-[(p-methylphenyl)thio]ethyl butyl ether (1609649-40-2)

Guidance literature:

With oxygen; copper(l) chloride; In dichloromethane; at 50 ℃; for 3h; Reagent/catalyst; Sealed tube;

DOI:10.1016/j.tet.2016.05.050

Reference yield: 99.0%

1-[(p-methylphenyl)thio]ethyl butyl ether (1609649-40-2) + para-thiocresol (106-45-6) → 1,1-bis<(4-methylphenyl)thio>ethane (33451-45-5)

Guidance literature:

With oxygen; copper(ll) bromide; at 50 ℃; for 3h; Mechanism; Sealed tube;

DOI:10.1016/j.tet.2016.05.050

upstream raw materials:

-butyl vinyl ether

para-thiocresol

Downstream raw materials:

1,1-bis<(4-methylphenyl)thio>ethane