Technology Process of 2,3-dioxo-5,10,15,20-tetramesitylchlorin
There total 7 articles about 2,3-dioxo-5,10,15,20-tetramesitylchlorin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxygen; silica gel;
In
dichloromethane;
for 2h;
UV-irradiation;
DOI:10.1039/c2dt32196c
- Guidance literature:
-
Multi-step reaction with 5 steps
2: dichloromethane
3: trifluoroacetic acid; sulfuric acid / dichloromethane / 2.5 h
4: sodium tetrahydroborate; palladium 10% on activated carbon / dichloromethane; methanol / 1 h / Inert atmosphere
5: oxygen; silica gel / dichloromethane / 2 h / UV-irradiation
With
sodium tetrahydroborate; sulfuric acid; palladium 10% on activated carbon; oxygen; silica gel; trifluoroacetic acid;
In
methanol; dichloromethane;
DOI:10.1039/c2dt32196c
- Guidance literature:
-
Multi-step reaction with 6 steps
1: boron trifluoride diethyl etherate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone / chloroform
3: dichloromethane
4: trifluoroacetic acid; sulfuric acid / dichloromethane / 2.5 h
5: sodium tetrahydroborate; palladium 10% on activated carbon / dichloromethane; methanol / 1 h / Inert atmosphere
6: oxygen; silica gel / dichloromethane / 2 h / UV-irradiation
With
sodium tetrahydroborate; sulfuric acid; palladium 10% on activated carbon; boron trifluoride diethyl etherate; oxygen; silica gel; triethylamine; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
methanol; dichloromethane; chloroform;
DOI:10.1039/c2dt32196c
