Technology Process of 2,4,6-Trimethylbenzaldehyde
There total 146 articles about 2,4,6-Trimethylbenzaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1,3,5-trimethyl-benzene;
With
titanium tetrachloride;
In
dichloromethane;
at 0 ℃;
for 1h;
Inert atmosphere;
Dichloromethyl methyl ether;
In
dichloromethane;
at 0 ℃;
for 0.75h;
regioselective reaction;
Inert atmosphere;
DOI:10.3390/molecules20045409
- Guidance literature:
-
With
rhodium(III) chloride trihydrate; hydrogen; triethylamine; triphenylphosphine;
In
N,N-dimethyl acetamide;
at 90 ℃;
for 12h;
under 7500.75 Torr;
Autoclave;
DOI:10.3762/bjoc.16.61
- Guidance literature:
-
2-hydroxy-2-(2,4,6-trimethylphenyl)acetonitrile;
With
(η(6)-benzene)chloro[1,2-bis(diphenylphosphino)ethane]ruthenium(II) chloride;
In
benzene;
at 120 ℃;
for 24h;
Inert atmosphere;
Schlenk technique;
With
water;
In
dichloromethane; ethyl acetate; benzene;
for 24h;
DOI:10.1002/adsc.201700786
Xi
