(1S,2R)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene diacetate

Base Information

Chemical Name:(1S,2R)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene diacetate
CAS No.:1259282-30-8
Molecular Formula:C₂₅H₃₀O₇
Molecular Weight:442.509
Hs Code.:

Synonyms:(1S,2R)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene diacetate

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Chemical Property of (1S,2R)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene diacetate

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Technology Process of (1S,2R)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene diacetate

There total 3 articles about (1S,2R)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1259282-29-5
(1S,2R)-2-allyl-1-(3,4-dimethoxyphenyl)trimethylene diacetate

: 5720-07-0
4-methoxyphenylboronic acid

: 1259282-30-8
(1S,2R)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene diacetate

Guidance literature:: With lithium acetate; copper diacetate; palladium diacetate; In N,N-dimethyl-formamide; at 100 ℃; for 2h;
DOI:10.1271/bbb.100255

Reference yield:

: 853750-45-5
(4S)-4-benzyl-3-{(2S)-2-[(S)-(3,4-dimethoxyphenyl)(hydroxy)methyl]-4-pentenoyl}-2-oxazolidinone

: 1259282-30-8
(1S,2R)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium borohydride / tetrahydrofuran; methanol / 1 h / 0 °C

2: pyridine / 5 h / 20 °C

3: lithium acetate; copper diacetate; palladium diacetate / N,N-dimethyl-formamide / 2 h / 100 °C

With pyridine; lithium borohydride; lithium acetate; copper diacetate; palladium diacetate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; 3: Mizoroki-Heck reaction;
DOI:10.1271/bbb.100255

Reference yield:

: C₁₄H₂₀O₄

: 1259282-30-8
(1S,2R)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 5 h / 20 °C

2: lithium acetate; copper diacetate; palladium diacetate / N,N-dimethyl-formamide / 2 h / 100 °C

With pyridine; lithium acetate; copper diacetate; palladium diacetate; In N,N-dimethyl-formamide; 2: Mizoroki-Heck reaction;
DOI:10.1271/bbb.100255