(1R,3S,5R)-5-(2-tert-Butoxycarbonylamino-ethylcarbamoyl)-1,3,5-trimethyl-cyclohexane-1,3-dicarboxylic acid

Base Information

Chemical Name:(1R,3S,5R)-5-(2-tert-Butoxycarbonylamino-ethylcarbamoyl)-1,3,5-trimethyl-cyclohexane-1,3-dicarboxylic acid
CAS No.:167017-70-1
Molecular Formula:C₁₉H₃₂N₂O₇
Molecular Weight:400.472
Hs Code.:

Synonyms:(1R,3S,5R)-5-(2-tert-Butoxycarbonylamino-ethylcarbamoyl)-1,3,5-trimethyl-cyclohexane-1,3-dicarboxylic acid

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Chemical Property of (1R,3S,5R)-5-(2-tert-Butoxycarbonylamino-ethylcarbamoyl)-1,3,5-trimethyl-cyclohexane-1,3-dicarboxylic acid

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Technology Process of (1R,3S,5R)-5-(2-tert-Butoxycarbonylamino-ethylcarbamoyl)-1,3,5-trimethyl-cyclohexane-1,3-dicarboxylic acid

There total 2 articles about (1R,3S,5R)-5-(2-tert-Butoxycarbonylamino-ethylcarbamoyl)-1,3,5-trimethyl-cyclohexane-1,3-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 57260-73-8
N-BOC-1,2-diaminoethane

: 107271-36-3
1,5,7-trimethyl-2,4-dioxo-3-oxabicyclo[3.3.1]nonane-7-carboxylic acid

: 167017-70-1
(1R,3S,5R)-5-(2-tert-Butoxycarbonylamino-ethylcarbamoyl)-1,3,5-trimethyl-cyclohexane-1,3-dicarboxylic acid

Guidance literature:: In N,N-dimethyl-formamide; for 6h; Ambient temperature;
DOI:10.1016/00404-0399(50)1370-W

Reference yield:

: tert-butyl (2-aminoethyl)carbamate hydrochloride

: 79410-20-1
Kemp's triacid

: 167017-70-1
(1R,3S,5R)-5-(2-tert-Butoxycarbonylamino-ethylcarbamoyl)-1,3,5-trimethyl-cyclohexane-1,3-dicarboxylic acid

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1039/c7cc03055j

Reference yield: 56.0%

: 4244-84-2
ethyl β-alaninate hydrochloride

: 167017-70-1
(1R,3S,5R)-5-(2-tert-Butoxycarbonylamino-ethylcarbamoyl)-1,3,5-trimethyl-cyclohexane-1,3-dicarboxylic acid

: C₂₉H₅₀N₄O₉

Guidance literature:: With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c7cc03055j