5-Benzyl-2-(3-trifluoromethyl-phenyl)-5H-pyrrolo[3,4-c]pyrrole-1,3-dione

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Chemical Name:5-Benzyl-2-(3-trifluoromethyl-phenyl)-5H-pyrrolo[3,4-c]pyrrole-1,3-dione
CAS No.:86732-07-2
Molecular Formula:C₂₀H₁₃F₃N₂O₂
Molecular Weight:370.331
Hs Code.:

Synonyms:5-Benzyl-2-(3-trifluoromethyl-phenyl)-5H-pyrrolo[3,4-c]pyrrole-1,3-dione

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Chemical Property of 5-Benzyl-2-(3-trifluoromethyl-phenyl)-5H-pyrrolo[3,4-c]pyrrole-1,3-dione

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Technology Process of 5-Benzyl-2-(3-trifluoromethyl-phenyl)-5H-pyrrolo[3,4-c]pyrrole-1,3-dione

There total 4 articles about 5-Benzyl-2-(3-trifluoromethyl-phenyl)-5H-pyrrolo[3,4-c]pyrrole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 680-31-9
N,N,N,N,N,N-hexamethylphosphoric triamide

: 86731-97-7
1-Benzyl-4-(3-trifluoromethyl-phenylcarbamoyl)-1H-pyrrole-3-carboxylic acid

: 86732-07-2
5-Benzyl-2-(3-trifluoromethyl-phenyl)-5H-pyrrolo[3,4-c]pyrrole-1,3-dione

: 86732-41-4
1-benzyl-3-dimethylcarbamoyl-4-(trifluoromethylphenyl)carbamoyl-1H-pyrrole

Guidance literature:: With thionyl chloride; Yield given. Multistep reaction; 1.) benzene, reflux, 1.5 h; 2.) 180 deg C;

Reference yield: 9.0%

: 86731-97-7
1-Benzyl-4-(3-trifluoromethyl-phenylcarbamoyl)-1H-pyrrole-3-carboxylic acid

: 86732-07-2
5-Benzyl-2-(3-trifluoromethyl-phenyl)-5H-pyrrolo[3,4-c]pyrrole-1,3-dione

: 86732-41-4
1-benzyl-3-dimethylcarbamoyl-4-(trifluoromethylphenyl)carbamoyl-1H-pyrrole

Guidance literature:: With thionyl chloride; Yield given. Multistep reaction; 1.) benzene, reflux, 1.5 h; 2.) hexamethylphosphoramide, 180 deg C;

Reference yield:

: 86731-90-0
1-benzyl-pyrrole-3,4-dicarboxylic acid

: 86732-07-2
5-Benzyl-2-(3-trifluoromethyl-phenyl)-5H-pyrrolo[3,4-c]pyrrole-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / dicyclohexylcarbodiimide / tetrahydrofuran / Heating; overnight

2: 76 percent / tetrahydrofuran

3: 83 percent / 1.) SOCl₂ / 1.) benzene, reflux, 1.5 h; 2.) 180 deg C

With thionyl chloride; dicyclohexyl-carbodiimide; In tetrahydrofuran;