ethyl cis-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-1-methylcyclohexanecarboxylate

Base Information

Chemical Name:ethyl cis-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-1-methylcyclohexanecarboxylate
CAS No.:1354806-09-9
Molecular Formula:C₁₆H₂₄O₆
Molecular Weight:312.363
Hs Code.:

Synonyms:ethyl cis-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-1-methylcyclohexanecarboxylate

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Chemical Property of ethyl cis-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-1-methylcyclohexanecarboxylate

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Technology Process of ethyl cis-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-1-methylcyclohexanecarboxylate

There total 4 articles about ethyl cis-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-1-methylcyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2033-24-1
cycl-isopropylidene malonate

: 147905-77-9
ethyl 1-methyl-4-oxo-1-cyclohexanecarboxylate

: 1400674-68-1
ethyl trans-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-1-methylcyclohexanecarboxylate

: 1354806-09-9
ethyl cis-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-1-methylcyclohexanecarboxylate

Guidance literature:: With sodium tris(acetoxy)borohydride; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

Reference yield:

: 17159-79-4
ethyl 4-oxocyclohexane-1-carboxylate

: 1354806-09-9
ethyl cis-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-1-methylcyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / toluene / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.42 h / -30 °C

2.2: 1.08 h / -5 - 23 °C

3.1: hydrogenchloride / water; acetone / 20 °C

4.1: sodium tris(acetoxy)borohydride / N,N-dimethyl-formamide / 4 h / 20 °C

With hydrogenchloride; sodium tris(acetoxy)borohydride; toluene-4-sulfonic acid; lithium diisopropyl amide; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: 1489-97-0
ethyl 1,4-dioxaspiro[4.5]decane-8-carboxylate

: 1354806-09-9
ethyl cis-4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)-1-methylcyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.42 h / -30 °C

1.2: 1.08 h / -5 - 23 °C

2.1: hydrogenchloride / water; acetone / 20 °C

3.1: sodium tris(acetoxy)borohydride / N,N-dimethyl-formamide / 4 h / 20 °C

With hydrogenchloride; sodium tris(acetoxy)borohydride; lithium diisopropyl amide; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone;