2',3',5'-tri-O-acetyl-8-bromo-O²,O⁶-bis<2-(p-nitrophenyl)ethyl>xanthosine

Base Information

Chemical Name:2',3',5'-tri-O-acetyl-8-bromo-O²,O⁶-bis<2-(p-nitrophenyl)ethyl>xanthosine
CAS No.:102562-11-8
Molecular Formula:C₃₂H₃₁BrN₆O₁₃
Molecular Weight:787.535
Hs Code.:

2',3',5'-tri-O-acetyl-8-bromo-O<sup>2</sup>,O<sup>6</sup>-bis<2-(p-nitrophenyl)ethyl>xanthosine

Synonyms:2',3',5'-tri-O-acetyl-8-bromo-O²,O⁶-bis<2-(p-nitrophenyl)ethyl>xanthosine

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Chemical Property of 2',3',5'-tri-O-acetyl-8-bromo-O²,O⁶-bis<2-(p-nitrophenyl)ethyl>xanthosine

Chemical Property:

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Technology Process of 2',3',5'-tri-O-acetyl-8-bromo-O²,O⁶-bis<2-(p-nitrophenyl)ethyl>xanthosine

There total 5 articles about 2',3',5'-tri-O-acetyl-8-bromo-O²,O⁶-bis<2-(p-nitrophenyl)ethyl>xanthosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 20264-96-4
2-(4-nitrophenyl)ethyl iodide

: 102604-04-6
2',3',5'-tri-O-acetyl-8-bromo-O⁶-<2-(p-nitrophenyl)ethyl>xanthosine

: 102562-11-8
2',3',5'-tri-O-acetyl-8-bromo-O²,O⁶-bis<2-(p-nitrophenyl)ethyl>xanthosine

Guidance literature:: silver (I) ion;
DOI:10.1016/S0040-4039(00)98224-8

Reference yield:

: 100-27-6
2-(4-nitrophenyl)ethanol

: 102562-11-8
2',3',5'-tri-O-acetyl-8-bromo-O²,O⁶-bis<2-(p-nitrophenyl)ethyl>xanthosine

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / triphenylphosphane, diethyl azodicarboxylate / dioxane / 1 h / Ambient temperature

2: 93 percent / NaNO₂, HClO₄ / acetone; H₂O / 1 h / 10 °C

3: 90 percent / Ag₂CO₃ / 1 h / Heating

With perchloric acid; triphenylphosphine; sodium nitrite; diethylazodicarboxylate; silver carbonate; In 1,4-dioxane; water; acetone;
DOI:10.1002/hlca.19870700126

Reference yield:

: 102604-08-0
2',3',5'-tri-O-acetyl-8-bromo-O⁶-<2(-p-nitrophenyl)ethyl>guanosine

: 102562-11-8
2',3',5'-tri-O-acetyl-8-bromo-O²,O⁶-bis<2-(p-nitrophenyl)ethyl>xanthosine

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NaNO₂, HClO₄ / acetone; H₂O / 1 h / 10 °C

2: 90 percent / Ag₂CO₃ / 1 h / Heating

With perchloric acid; sodium nitrite; silver carbonate; In water; acetone;
DOI:10.1002/hlca.19870700126