3-β-cholestanyl trimethylsilyl ether

Base Information

• Chemical Name: 3-β-cholestanyl trimethylsilyl ether
• CAS No.: 42995-55-1
• Molecular Formula: C₃₀H₅₆OSi
• Molecular Weight: 460.86
• Mol file: 42995-55-1.mol

Synonyms:3-β-cholestanyl trimethylsilyl ether

Chemical Property of 3-β-cholestanyl trimethylsilyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-β-cholestanyl trimethylsilyl ether

There total 3 articles about 3-β-cholestanyl trimethylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Coprostanol (80-97-7,360-68-9,516-92-7,516-95-0,566-84-7,14615-12-4,16720-60-8,17608-41-2,18769-46-5,27409-41-2,56193-35-2,57759-49-6,73465-18-6,103365-91-9,105119-51-5) + N,O-Bis(trimethylsilyl)trifluoroacetamide (25561-30-2) → 3β-trimethylsilyloxy-5β-cholestan (18880-50-7,18880-51-8,42995-55-1,47701-87-1,47701-88-2,55331-93-6,55331-94-7,56907-47-2)

Guidance literature:

In hexane; at 37 ℃; for 2h;

DOI:10.1016/j.bmc.2012.05.003

Reference yield:

→ Coprostanyltrimethylsilylether (18880-50-7,18880-51-8,42995-55-1,47701-87-1,47701-88-2,55331-93-6,55331-94-7,56907-47-2)

Guidance literature:

Mensche. Exkrementen mit Hexamethyldisilazan;

Reference yield:

→ 5α-Cholestan-3β-ol-trimethylsilylaether (18880-50-7,18880-51-8,42995-55-1,47701-87-1,47701-88-2,55331-93-6,55331-94-7,56907-47-2)

Guidance literature:

5α-Cholestan-3β-ol, Trimethylsilylchlorid in Py.;

upstream raw materials:

Coprostanol

N,O-Bis(trimethylsilyl)trifluoroacetamide

Downstream raw materials:

3β-cholestanyl 2,3,5-tri-O-benzyl-β-D-ribofuranoside

{(2R,3R,4R,5S,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-[(3S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yloxy]-tetrahydro-pyran-3-yl}-carbamic acid benzyl ester

(2R,3R,4S)-3,4-Bis-benzyloxy-2-benzyloxymethyl-5-[(3S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yloxy]-tetrahydro-furan

(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-[(3S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yloxy]-tetrahydro-pyran