Technology Process of C17H18S2
There total 3 articles about C17H18S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridinium chlorochromate / dichloromethane / 20 °C / Inert atmosphere; Molecular sieve
2: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere
With
boron trifluoride diethyl etherate; pyridinium chlorochromate;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium tetrahydroborate; iodine / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux
1.2: 0 - 20 °C
2.1: pyridinium chlorochromate / dichloromethane / 20 °C / Inert atmosphere; Molecular sieve
3.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere
With
sodium tetrahydroborate; boron trifluoride diethyl etherate; iodine; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane;