2-O-benzyl-1-N-[2-(R)-O-benzyl-4-benzyloxycarbonylaminobutyryl]-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxy-2-hydroxyneamine

Base Information

Chemical Name:2-O-benzyl-1-N-[2-(R)-O-benzyl-4-benzyloxycarbonylaminobutyryl]-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxy-2-hydroxyneamine
CAS No.:959919-09-6
Molecular Formula:C₆₂H₆₉N₅O₁₅
Molecular Weight:1124.25
Hs Code.:

Synonyms:2-O-benzyl-1-N-[2-(R)-O-benzyl-4-benzyloxycarbonylaminobutyryl]-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxy-2-hydroxyneamine

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Chemical Property of 2-O-benzyl-1-N-[2-(R)-O-benzyl-4-benzyloxycarbonylaminobutyryl]-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxy-2-hydroxyneamine

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Technology Process of 2-O-benzyl-1-N-[2-(R)-O-benzyl-4-benzyloxycarbonylaminobutyryl]-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxy-2-hydroxyneamine

There total 1 articles about 2-O-benzyl-1-N-[2-(R)-O-benzyl-4-benzyloxycarbonylaminobutyryl]-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxy-2-hydroxyneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 959919-11-0
(R)-2-benzyloxy-4-benzyloxycarbonylaminobutyric acid

: 959918-81-1
2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine

: 959919-09-6
2-O-benzyl-1-N-[2-(R)-O-benzyl-4-benzyloxycarbonylaminobutyryl]-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxy-2-hydroxyneamine

Guidance literature:: With 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In tetrahydrofuran; water; isopropyl alcohol; at 20 ℃; for 5.5h;

Reference yield:

: 959918-87-7
4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose

: 959919-09-6
2-O-benzyl-1-N-[2-(R)-O-benzyl-4-benzyloxycarbonylaminobutyryl]-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxy-2-hydroxyneamine

: 4,6-di-O-acetyl-2,2-di-O-benzyl-1-N-[2-(R)-O-benzyl-4-benzyloxycarbonylaminobutyryl]-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

Guidance literature:: 4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose; 2-O-benzyl-1-N-[2-(R)-O-benzyl-4-benzyloxycarbonylaminobutyryl]-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxy-2-hydroxyneamine; In dichloromethane; at 20 ℃; for 2h; Molecular sieve;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -20 - 20 ℃; for 4h; light shielding;

With triethylamine; In dichloromethane; at 0 ℃;