4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose

Base Information

Chemical Name:4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose
CAS No.:959918-87-7
Molecular Formula:C₃₁H₃₃NO₈S
Molecular Weight:579.671
Hs Code.:

Synonyms:4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose

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Chemical Property of 4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose

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Technology Process of 4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose

There total 1 articles about 4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 959918-86-6
2-O-Benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose

: 108-24-7
acetic anhydride

: 959918-87-7
4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose

Guidance literature:: With pyridine; at 0 - 20 ℃; for 3 - 16h; Product distribution / selectivity;

Reference yield: 68.0%

: 959918-87-7
4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose

: 959918-82-2
1-N-[(S)-4-benzyloxycarbonylamino-2-benzyloxybutylyl]-2-benzyloxy-3,2′,6′-tris(N-benzyloxycarbonyl)-3′,4′-dideoxyneamine

: 959918-88-8
C₈₇H₉₆N₆O₂₃

Guidance literature:: 4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose; 1-N-[(S)-4-benzyloxycarbonylamino-2-benzyloxybutylyl]-2-benzyloxy-3,2′,6′-tris(N-benzyloxycarbonyl)-3′,4′-dideoxyneamine; In dichloromethane; at 20 ℃; for 1h; Molecular sieve;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -15 - 20 ℃; for 1.66 - 4h; light shielding;

With triethylamine; In dichloromethane; at 0 ℃; Product distribution / selectivity;

Reference yield:

: 959918-87-7
4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose

: 959919-03-0
1-N-[(S)-6-amino-2-benzyloxy-N-benzyloxycarbonylhexanoyl]-2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine

: 959919-06-3
4,6-di-O-acetyl-1-N-[(S)-6-amino-2-benzyloxy-N-benzyloxycarbonylhexanoyl]-2,2-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

Guidance literature:: 4,6-Di-O-acetyl-2-O-benzyl-3-benzyloxycarbonylamino-1,3-dideoxy-1-phenylthio-α-D-glucopyranose; 1-N-[(S)-6-amino-2-benzyloxy-N-benzyloxycarbonylhexanoyl]-2-benzyloxy-3,2',6'-tri-N-benzyloxycarbonyl-3',4'-dideoxyneamine; In dichloromethane; at 20 ℃; for 1h; Molecular sieve;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -20 - 20 ℃; for 3h; light shielding;

With triethylamine; In dichloromethane; at 0 ℃;