(2R,3R,4R)-1,3-O-(S)-benzylidene-2-O-methanesulfonyl-5-phenyl-1,2,3,4-pentanetetrol

Base Information

Chemical Name:(2R,3R,4R)-1,3-O-(S)-benzylidene-2-O-methanesulfonyl-5-phenyl-1,2,3,4-pentanetetrol
CAS No.:1375103-29-9
Molecular Formula:C₁₉H₂₂O₆S
Molecular Weight:378.446
Hs Code.:

Synonyms:(2R,3R,4R)-1,3-O-(S)-benzylidene-2-O-methanesulfonyl-5-phenyl-1,2,3,4-pentanetetrol

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Chemical Property of (2R,3R,4R)-1,3-O-(S)-benzylidene-2-O-methanesulfonyl-5-phenyl-1,2,3,4-pentanetetrol

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Technology Process of (2R,3R,4R)-1,3-O-(S)-benzylidene-2-O-methanesulfonyl-5-phenyl-1,2,3,4-pentanetetrol

There total 3 articles about (2R,3R,4R)-1,3-O-(S)-benzylidene-2-O-methanesulfonyl-5-phenyl-1,2,3,4-pentanetetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1375103-39-1
C₁₈H₂₀O₄

: 124-63-0
methanesulfonyl chloride

: 1375103-29-9
(2R,3R,4R)-1,3-O-(S)-benzylidene-2-O-methanesulfonyl-5-phenyl-1,2,3,4-pentanetetrol

Guidance literature:: With pyridine; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2012.03.025

Reference yield:

: 591-51-5
phenyllithium

: 1375103-29-9
(2R,3R,4R)-1,3-O-(S)-benzylidene-2-O-methanesulfonyl-5-phenyl-1,2,3,4-pentanetetrol

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) iodide / tetrahydrofuran / 6 h / -40 - 20 °C

1.2: Saturated solution

2.1: pyridine / 0 - 20 °C

With pyridine; copper(l) iodide; In tetrahydrofuran;
DOI:10.1016/j.bmc.2012.03.025

Reference yield:

: 164576-09-4
4,5-anhydro-1,3-O-benzylidene-D-arabinitol

: 1375103-29-9
(2R,3R,4R)-1,3-O-(S)-benzylidene-2-O-methanesulfonyl-5-phenyl-1,2,3,4-pentanetetrol

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) iodide / tetrahydrofuran / 6 h / -40 - 20 °C

1.2: Saturated solution

2.1: pyridine / 0 - 20 °C

With pyridine; copper(l) iodide; In tetrahydrofuran;
DOI:10.1016/j.bmc.2012.03.025