4-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-D-erythrose diethyl dithioacetal

Base Information

Chemical Name:4-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-D-erythrose diethyl dithioacetal
CAS No.:105265-86-9
Molecular Formula:C₂₇H₄₀O₃S₂Si
Molecular Weight:504.83
Hs Code.:

Synonyms:4-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-D-erythrose diethyl dithioacetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-D-erythrose diethyl dithioacetal

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Technology Process of 4-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-D-erythrose diethyl dithioacetal

There total 3 articles about 4-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-D-erythrose diethyl dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108714-02-9
(2R,3R)-4-(tert-butyl-diphenyl-silanyloxy)-1,1-bisethylsulfanyl-butane-2,3-diol

: 77-76-9
2,2-dimethoxy-propane

: 105265-86-9
4-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-D-erythrose diethyl dithioacetal

Guidance literature:: With (1S)-10-camphorsulfonic acid; In acetone; for 4h; Ambient temperature;
DOI:10.1021/jo00386a011

Reference yield:

: 51295-44-4
D-erythrose diethyl dithioacetal

: 105265-86-9
4-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-D-erythrose diethyl dithioacetal

Guidance literature:: Multi-step reaction with 2 steps

2: TsOH / acetone

With toluene-4-sulfonic acid; In acetone;
DOI:10.1246/cl.1986.1081

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 105265-86-9
4-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-D-erythrose diethyl dithioacetal

Guidance literature:: Multi-step reaction with 2 steps

2: TsOH / acetone

With toluene-4-sulfonic acid; In acetone;
DOI:10.1246/cl.1986.1081