H-Phe-NH-iC₄H₉

Base Information

• Chemical Name: H-Phe-NH-iC₄H₉
• CAS No.: 108050-51-7
• Molecular Formula: C₁₃H₂₀N₂O
• Molecular Weight: 220.315

Synonyms:H-Phe-NH-iC₄H₉

Chemical Property of H-Phe-NH-iC₄H₉

Chemical Property:

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Technology Process of H-Phe-NH-iC₄H₉

There total 7 articles about H-Phe-NH-iC₄H₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C21H26N2O3 (911289-39-9) → H-Phe-NH-iC4H9 (108050-51-7)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 15h;

DOI:10.1039/d1ob01565f

Reference yield: 80.0%

N-tert-butoxycarbonyl-L-phenylalanine (13734-34-4) + isobutylamine (78-81-9) → H-Phe-NH-iC4H9 (108050-51-7)

Guidance literature:

With EDAC; benzotriazol-1-ol; trifluoroacetic acid; In N,N-dimethyl-formamide;

Reference yield: 29.0%

isobutylamine (78-81-9) + L-Phe-BF2 → H-Phe-NH-iC4H9 (108050-51-7)

Guidance literature:

DOI:10.1016/j.tetlet.2004.11.129

upstream raw materials:

isobutylamine

N-tert-butoxycarbonyl-L-phenylalanine

C₂₁H₂₆N₂O₃

N-Cbz-L-Phe

Downstream raw materials:

C₃₃H₃₅N₃O₄

C₁₉H₂₃N₃O₄*ClH

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