N-<(tert-butoxycarbonyl)-L-valinyl>-N-benzyl-N-(2-acetoxy-5-nitrobenzyl)amide

Base Information

Chemical Name:N-<(tert-butoxycarbonyl)-L-valinyl>-N-benzyl-N-(2-acetoxy-5-nitrobenzyl)amide
CAS No.:75830-36-3
Molecular Formula:C₂₆H₃₃N₃O₇
Molecular Weight:499.564
Hs Code.:

Synonyms:N-<(tert-butoxycarbonyl)-L-valinyl>-N-benzyl-N-(2-acetoxy-5-nitrobenzyl)amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<(tert-butoxycarbonyl)-L-valinyl>-N-benzyl-N-(2-acetoxy-5-nitrobenzyl)amide

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Technology Process of N-<(tert-butoxycarbonyl)-L-valinyl>-N-benzyl-N-(2-acetoxy-5-nitrobenzyl)amide

There total 6 articles about N-<(tert-butoxycarbonyl)-L-valinyl>-N-benzyl-N-(2-acetoxy-5-nitrobenzyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 108-24-7
acetic anhydride

: {1-[Benzyl-(2-hydroxy-5-nitro-benzyl)-carbamoyl]-2-methyl-propyl}-carbamic acid tert-butyl ester

: 75830-36-3
N-<(tert-butoxycarbonyl)-L-valinyl>-N-benzyl-N-(2-acetoxy-5-nitrobenzyl)amide

Guidance literature:: In pyridine; at 2 ℃; for 24h;
DOI:10.1021/jo00316a003

Reference yield:

: 53848-16-1
5-nitrosalicylaldehyde benzylamine Schiff base

: 75830-36-3
N-<(tert-butoxycarbonyl)-L-valinyl>-N-benzyl-N-(2-acetoxy-5-nitrobenzyl)amide

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄, HCl

2: sodium hydroxide / H₂O

3: N-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide / 24 h / 25 °C

4: 80 percent / pyridine / 24 h / 2 °C

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In pyridine; water; N,N-dimethyl-formamide;
DOI:10.1021/jo00316a003

Reference yield:

: 75830-37-4
N-(2-hydroxy-5-nitrobenzyl)benzylamine*HCl

: 75830-36-3
N-<(tert-butoxycarbonyl)-L-valinyl>-N-benzyl-N-(2-acetoxy-5-nitrobenzyl)amide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / H₂O

2: N-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide / 24 h / 25 °C

3: 80 percent / pyridine / 24 h / 2 °C

With sodium hydroxide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In pyridine; water; N,N-dimethyl-formamide;
DOI:10.1021/jo00316a003