C₂₁H₂₅NO₂

Base Information

Chemical Name:C₂₁H₂₅NO₂
CAS No.:1309678-90-7
Molecular Formula:C₂₁H₂₅NO₂
Molecular Weight:323.435
Hs Code.:

C<sub>21</sub>H<sub>25</sub>NO<sub>2</sub>

Synonyms:C₂₁H₂₅NO₂

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Chemical Property of C₂₁H₂₅NO₂

Chemical Property:

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Technology Process of C₂₁H₂₅NO₂

There total 6 articles about C₂₁H₂₅NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1309678-67-8
(2S,3R,4S,5R,6S)-ethyl 5-methyl-3-phenethyl-6-phenyl-7-oxa-1-azabicyclo[2.2.1]-heptane-2-carboxylate

: 1309678-90-7
C₂₁H₂₅NO₂

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 0.0166667h; Inert atmosphere;
DOI:10.1021/ja202900h

Reference yield:

: 1309678-95-2
C₁₉H₂₃NO

: 1309678-90-7
C₂₁H₂₅NO₂

Guidance literature:: Multi-step reaction with 2 steps

1: water; toluene / 12 h / 100 °C / Molecular sieve; Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 0.02 h / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; In tetrahydrofuran; water; toluene;
DOI:10.1021/ja202900h

Reference yield:

: 1016652-30-4
(S)-(Z)-1-phenyl-4-hexen-3-ol

: 1309678-90-7
C₂₁H₂₅NO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran; diethyl ether / -10 °C / Inert atmosphere

1.2: 0.08 h / Inert atmosphere

2.1: dipotassium hydrogenphosphate / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

3.1: hydrazine hydrate / ethanol / 4 h / 20 °C / Inert atmosphere

4.1: water; toluene / 12 h / 100 °C / Molecular sieve; Inert atmosphere

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.02 h / 0 °C / Inert atmosphere

With dipotassium hydrogenphosphate; lithium aluminium tetrahydride; hydrazine hydrate; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; ethanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja202900h