C₂₆H₄₈O₅Si₂

Base Information

Chemical Name:C₂₆H₄₈O₅Si₂
CAS No.:1395502-76-7
Molecular Formula:C₂₆H₄₈O₅Si₂
Molecular Weight:496.835
Hs Code.:

C<sub>26</sub>H<sub>48</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₂₆H₄₈O₅Si₂

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Chemical Property of C₂₆H₄₈O₅Si₂

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Technology Process of C₂₆H₄₈O₅Si₂

There total 6 articles about C₂₆H₄₈O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1395502-75-6
C₂₆H₅₀O₅Si₂

: 1395502-76-7
C₂₆H₄₈O₅Si₂

Guidance literature:: With sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine; In dichloromethane; dimethyl sulfoxide; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/ol302072b

Reference yield:

: 1395502-34-7
C₁₅H₂₀O₄

: 1395502-76-7
C₂₆H₄₈O₅Si₂

Guidance literature:: Multi-step reaction with 4 steps

1: AD-mix-α; methanesulfonamide / 1,4-dioxane; water / 48 h / 0 °C / Inert atmosphere

2: pyridine; silver nitrate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C / Inert atmosphere

4: N-ethyl-N,N-diisopropylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1.5 h / 20 °C / Inert atmosphere

With pyridine; methanesulfonamide; AD-mix-α; sulfur trioxide pyridine complex; diisobutylaluminium hydride; silver nitrate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ol302072b

Reference yield:

: 170649-28-2
(3S)-3-<(p-methoxybenzyl)-oxy>-butanal

: 1395502-76-7
C₂₆H₄₈O₅Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: toluene / 5 h / 80 °C / Inert atmosphere

2: AD-mix-α; methanesulfonamide / 1,4-dioxane; water / 48 h / 0 °C / Inert atmosphere

3: pyridine; silver nitrate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

4: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C / Inert atmosphere

5: N-ethyl-N,N-diisopropylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1.5 h / 20 °C / Inert atmosphere

With pyridine; methanesulfonamide; AD-mix-α; sulfur trioxide pyridine complex; diisobutylaluminium hydride; silver nitrate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; 1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/ol302072b