Boc-Trp-Phe-NH₂

Base Information

Chemical Name:Boc-Trp-Phe-NH₂
CAS No.:33900-27-5
Molecular Formula:C₂₅H₃₀N₄O₄
Molecular Weight:450.538
Hs Code.:

Synonyms:Boc-Trp-Phe-NH₂

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Chemical Property of Boc-Trp-Phe-NH₂

Chemical Property:

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Technology Process of Boc-Trp-Phe-NH₂

There total 5 articles about Boc-Trp-Phe-NH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 47355-10-2
Nα-tert-butoxycarbonyl-1-formyl-L-tryptophan

: 33900-27-5
Boc-Trp-Phe-NH₂

Guidance literature:: N-tert-butoxycarbonyl-L-phenylalanine; With 1,1'-carbonyldiimidazole; In acetonitrile;

With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 50 ℃; for 18h; Inert atmosphere;

Nα-tert-butoxycarbonyl-1-formyl-L-tryptophan; Further stages;
DOI:10.1016/j.bmc.2010.06.053

Reference yield:

: 65864-22-4
(S)-2-amino-3-phenylpropionamide hydrochloride

: 13139-14-5
Boc-Trp-OH

: 33900-27-5
Boc-Trp-Phe-NH₂

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; at 0 ℃; for 12h;
DOI:10.1039/b301507f

Reference yield:

: 13139-14-5
Boc-Trp-OH

: 81092-89-9
L-phenylalanine amide trifluoroacetate

: 33900-27-5
Boc-Trp-Phe-NH₂

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In chloroform; N,N-dimethyl-formamide; at 0 ℃; for 8h;
DOI:10.1039/b306161m