3-chloro-N-hexylaniline

Base Information

Chemical Name:3-chloro-N-hexylaniline
CAS No.:1040324-87-5
Molecular Formula:C₁₂H₁₈ClN
Molecular Weight:211.735
Hs Code.:

Synonyms:3-chloro-N-hexylaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-chloro-N-hexylaniline

Chemical Property:

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Technology Process of 3-chloro-N-hexylaniline

There total 1 articles about 3-chloro-N-hexylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 108-37-2
1-bromo-3-chlorobenzene

: 111-26-2
hexan-1-amine

: 1040324-87-5
3-chloro-N-hexylaniline

Guidance literature:: With dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; sodium t-butanolate; In toluene; at 110 ℃; for 18h; Inert atmosphere;
DOI:10.1002/anie.201208544

Reference yield: 73.0%

: 1040324-87-5
3-chloro-N-hexylaniline

: 100-52-7
benzaldehyde

: (E)-3-(2-benzylidenehydrazinyl)-N-hexylaniline

Guidance literature:: 3-chloro-N-hexylaniline; With chloro[2-(dicyclohexylphosphino)-3 ,6-dimethoxy-2’,4’, 6’-triisopropyl- 1,1’-biphenyl] [2-(2-aminoethyl)phenyl]palladium(II); sodium t-butanolate; hydrazine; In tetrahydrofuran; at 20 ℃; for 0.05h; Flow reactor; Sonication; Inert atmosphere;

benzaldehyde; With trifluoroacetic acid; In tetrahydrofuran-d8; water; at 60 ℃; for 0.1h; Flow reactor; Sonication; Inert atmosphere;
DOI:10.1002/anie.201208544

Reference yield: 66.0%

: 1040324-87-5
3-chloro-N-hexylaniline

: 7152-15-0
ethyl 4-methyl-3-oxo-pentanoate

: 1-(3-(hexylamino)phenyl)-3-isopropyl-1H-pyrazol-5(4H)-one

Guidance literature:: 3-chloro-N-hexylaniline; With chloro[2-(dicyclohexylphosphino)-3 ,6-dimethoxy-2’,4’, 6’-triisopropyl- 1,1’-biphenyl] [2-(2-aminoethyl)phenyl]palladium(II); sodium t-butanolate; hydrazine; In tetrahydrofuran; at 20 ℃; for 0.05h; Flow reactor; Sonication; Inert atmosphere;

ethyl 4-methyl-3-oxo-pentanoate; With trifluoroacetic acid; In tetrahydrofuran-d8; water; at 125 ℃; for 0.25h; Flow reactor; Sonication; Inert atmosphere;
DOI:10.1002/anie.201208544