dimethyl -2-cyclohexenyl>allylmalonate

Base Information

Chemical Name:dimethyl -2-cyclohexenyl>allylmalonate
CAS No.:136569-44-3
Molecular Formula:C₁₉H₂₆O₈
Molecular Weight:382.411
Hs Code.:

dimethyl <trans-4-<(dimethoxycarbonyl)methyl>-2-cyclohexenyl>allylmalonate

Synonyms:dimethyl -2-cyclohexenyl>allylmalonate

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Chemical Property of dimethyl -2-cyclohexenyl>allylmalonate

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Technology Process of dimethyl -2-cyclohexenyl>allylmalonate

There total 3 articles about dimethyl -2-cyclohexenyl>allylmalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40637-56-7
dimethyl allylmalonate

: 136569-44-3
dimethyl -2-cyclohexenyl>allylmalonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1) DMF, 0 deg C to r.t., 2) 0 deg C to r.t., 16 h

2: 1) NaH, 2) Pd(dibenzylideneacetone)2, PPh₃ / 1) DMSO, 2 h, r.t, 2) 120 deg C, 3 h

With sodium hydride; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾;
DOI:10.1021/jo00022a004

Reference yield:

: 82736-39-8
cis-1-acetoxy-4-chlorocyclohex-2-ene

: 136569-44-3
dimethyl -2-cyclohexenyl>allylmalonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1) DMF, 0 deg C to r.t., 2) 0 deg C to r.t., 16 h

2: 1) NaH, 2) Pd(dibenzylideneacetone)2, PPh₃ / 1) DMSO, 2 h, r.t, 2) 120 deg C, 3 h

With sodium hydride; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾;
DOI:10.1021/jo00022a004

Reference yield:

: 113427-15-9,113427-17-1,121455-14-9,121455-17-2
trans-dimethyl 2-(4-acetoxycyclohex-2-enyl)-2-(prop-2-enyl)propanedioate

: 108-59-8
malonic acid dimethyl ester

: 136569-44-3
dimethyl -2-cyclohexenyl>allylmalonate

Guidance literature:: With sodium hydride; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; Yield given. Multistep reaction; 1) DMSO, 2 h, r.t, 2) 120 deg C, 3 h;
DOI:10.1021/jo00022a004