methyl 2,3-di-O-benzyl-6-O-p-methoxybenzyl-4-O-methyl-β-D-glucopyranoside

Base Information

Chemical Name:methyl 2,3-di-O-benzyl-6-O-p-methoxybenzyl-4-O-methyl-β-D-glucopyranoside
CAS No.:1403227-82-6
Molecular Formula:C₃₀H₃₆O₇
Molecular Weight:508.612
Hs Code.:

Synonyms:methyl 2,3-di-O-benzyl-6-O-p-methoxybenzyl-4-O-methyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,3-di-O-benzyl-6-O-p-methoxybenzyl-4-O-methyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of methyl 2,3-di-O-benzyl-6-O-p-methoxybenzyl-4-O-methyl-β-D-glucopyranoside

There total 5 articles about methyl 2,3-di-O-benzyl-6-O-p-methoxybenzyl-4-O-methyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 156881-26-4
methyl 2,3-di-O-benzyl-4,6-O-(4-methoxybenzyl)-β-D-glucopyranoside

: 74-88-4
methyl iodide

: 1403227-82-6
methyl 2,3-di-O-benzyl-6-O-p-methoxybenzyl-4-O-methyl-β-D-glucopyranoside

Guidance literature:: methyl 2,3-di-O-benzyl-4,6-O-(4-methoxybenzyl)-β-D-glucopyranoside; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; mineral oil; at 0 ℃;
DOI:10.1039/c2cc30805c

Reference yield:

: 709-50-2
methyl beta-D-glucopyranoside

: 1403227-82-6
methyl 2,3-di-O-benzyl-6-O-p-methoxybenzyl-4-O-methyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 5 h / 40 - 70 °C / 30 Torr

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

2.2: 0 - 20 °C

3.1: sodium cyanoborohydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

3.2: 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

4.2: 0 °C

With sodium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c2cc30805c

Reference yield:

: 1319723-49-3
methyl 4,6-O-p-methoxybenzylidene-2,3-di-O-benzyl-β-D-glucopyranoside

: 1403227-82-6
methyl 2,3-di-O-benzyl-6-O-p-methoxybenzyl-4-O-methyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium cyanoborohydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

1.2: 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

2.2: 0 °C

With sodium hydride; sodium cyanoborohydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c2cc30805c