6,7,8,9,10,11,17,18-Octahydro-5H-dibenzo(e,n)(1,4,8,12)dioxadiazacyclopentadecine

Base Information

Chemical Name:6,7,8,9,10,11,17,18-Octahydro-5H-dibenzo(e,n)(1,4,8,12)dioxadiazacyclopentadecine
CAS No.:65639-43-2
Molecular Formula:C19H24N2O2
Molecular Weight:312.412
Hs Code.:2934999090
European Community (EC) Number:265-848-8
DSSTox Substance ID:DTXSID40215878
Nikkaji Number:J307.446C
Mol file:65639-43-2.mol

Synonyms:65639-43-2;6,7,8,9,10,11,17,18-Octahydro-5H-dibenzo(e,n)(1,4,8,12)dioxadiazacyclopentadecine;5,6,14,15-Dibenzo-1,4-dioxa-8,12-diazacyclopentadeca-5,14-diene;EINECS 265-848-8;2,5-dioxa-13,17-diazatricyclo[17.4.0.06,11]tricosa-1(23),6,8,10,19,21-hexaene;5H-Dibenzo(e,n)(1,4,8,12)dioxadiazacyclopentadecine, 6,7,8,9,10,11,17,18-octahydro-;6,7,8,9,10,11,17,18-Octahydro-5H-dibenzo[e,n][1,4,8,12]dioxadiazacyclopentadecine;Dibenzodiaza-15-crown-4;SCHEMBL7534125;DTXSID40215878;AKOS015889609;FT-0701416;5,6,14,15-Dibenzo-1,4-dioxa-8,12-diazacyclopentadeca-5,14-diene, >=98.0% (NT)

Suppliers and Price of 6,7,8,9,10,11,17,18-Octahydro-5H-dibenzo(e,n)(1,4,8,12)dioxadiazacyclopentadecine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5,6,14,15-Dibenzo-1,4-dioxa-8,12-diazacyclopentadeca-5,14-diene
2.5g
$ 505.00

TRC
5,6,14,15-Dibenzo-1,4-dioxa-8,12-diazacyclopentadeca-5,14-diene
1g
$ 250.00

Sigma-Aldrich
5,6,14,15-Dibenzo-1,4-dioxa-8,12-diazacyclopentadeca-5,14-diene ≥98.0% (NT)
5g-f
$ 610.00

American Custom Chemicals Corporation
5,6,14,15-DIBENZO-1,4-DIOXA-8,12-DIAZACYCLOPENTADECA-5,14-DIENE 95.00%
5G
$ 1397.09

American Custom Chemicals Corporation
5,6,14,15-DIBENZO-1,4-DIOXA-8,12-DIAZACYCLOPENTADECA-5,14-DIENE 95.00%
1G
$ 758.57

Total 6 raw suppliers

Chemical Property of 6,7,8,9,10,11,17,18-Octahydro-5H-dibenzo(e,n)(1,4,8,12)dioxadiazacyclopentadecine

Chemical Property:

Vapor Pressure:1.63E-09mmHg at 25°C
Melting Point:142-144oC
Boiling Point:483.8°Cat760mmHg
Flash Point:202°C
PSA：42.52000
Density:1.041g/cm³
LogP:3.38490
XLogP3:2.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:312.183778013
Heavy Atom Count:23
Complexity:297

Purity/Quality:

99% ^*data from raw suppliers

5,6,14,15-Dibenzo-1,4-dioxa-8,12-diazacyclopentadeca-5,14-diene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: 22-24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:C1CNCC2=CC=CC=C2OCCOC3=CC=CC=C3CNC1
Uses 5,6,14,15-Dibenzo-1,4-dioxa-8,12-diazacyclopentadeca-5,14-diene is a mixed donor macrocyclic ligand.

Technology Process of 6,7,8,9,10,11,17,18-Octahydro-5H-dibenzo(e,n)(1,4,8,12)dioxadiazacyclopentadecine

There total 5 articles about 6,7,8,9,10,11,17,18-Octahydro-5H-dibenzo(e,n)(1,4,8,12)dioxadiazacyclopentadecine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52026-37-6
2,5-dioxa-13,17-diazatricyclo[17.4.0.0^6,11]tricosa-6,8,10,12,17,19,21,23⁽¹⁾-octaene

: 65639-43-2
6,7,8,9,10,11,17,18-octahydro-5H-dibenzo[e,n][1,4]dioxa[8,12]diazacyclopentadecine

Guidance literature:: With hydrogen; palladium on activated charcoal;

Reference yield:

: 66810-83-1
Ni(OenNtnH₄)Cl₂

: 65639-43-2
6,7,8,9,10,11,17,18-octahydro-5H-dibenzo[e,n][1,4]dioxa[8,12]diazacyclopentadecine

: 83864-14-6
nickel dichloride

Guidance literature:: With HClO₄ or HCl or; CF₃SO₃H or HNO₃ or; CH₃COOH; In water; Kinetics;
DOI:10.1021/ic50205a028

Reference yield:

: 90-02-8
salicylaldehyde

: 65639-43-2
6,7,8,9,10,11,17,18-octahydro-5H-dibenzo[e,n][1,4]dioxa[8,12]diazacyclopentadecine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol / Reflux

2: methanol / 0.33 h / Reflux

3: sodium tetrahydroborate / 20 °C

With sodium tetrahydroborate; sodium hydroxide; In methanol; ethanol;
DOI:10.1016/j.saa.2016.08.031