C₂₇H₂₈SO₃N₂

Base Information

Chemical Name:C₂₇H₂₈SO₃N₂
CAS No.:943439-58-5
Molecular Formula:C₂₇H₂₈N₂O₃S
Molecular Weight:460.597
Hs Code.:

C<sub>27</sub>H<sub>28</sub>SO<sub>3</sub>N<sub>2</sub>

Synonyms:C₂₇H₂₈SO₃N₂

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Chemical Property of C₂₇H₂₈SO₃N₂

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Technology Process of C₂₇H₂₈SO₃N₂

There total 8 articles about C₂₇H₂₈SO₃N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 943439-57-4
6-methoxy-3-{4-[2-(1-piperidinyl)ethoxy]phenoxy}-2-(4-aminophenyl)benzo[b]thiophene

: 943439-58-5
C₂₇H₂₈SO₃N₂

Guidance literature:: 6-methoxy-3-{4-[2-(1-piperidinyl)ethoxy]phenoxy}-2-(4-aminophenyl)benzo[b]thiophene; With hydrogenchloride; In diethyl ether; dichloromethane; at 20 ℃; for 0.5h;

With boron dimethyl-trifluoro sulphide; In dichloromethane; at 20 ℃; for 5h; Further stages.;
DOI:10.1021/jm070079j

Reference yield:

: 943439-53-0
6-methoxy-2-(4-bromophenyl)-3-bromobenzo[b]thiophene

: 943439-58-5
C₂₇H₂₈SO₃N₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 65 percent / TFA; aq. H₂O₂ / CH₂Cl₂ / 2 h / 20 °C

2.1: NaH / dimethylformamide / 0.33 h

2.2: 94 percent / dimethylformamide / 1 h / 20 °C

3.1: HCl / CH₂Cl₂; diethyl ether / 1 h

3.2: 85 percent / TMSCl; Ph₃P / tetrahydrofuran / 8 h / Heating

4.1: 74 percent / NaN₃; NaOH / CuI; L-proline / dimethylsulfoxide; ethanol / 10 h / 110 °C

5.1: HCl / CH₂Cl₂; diethyl ether / 0.5 h / 20 °C

5.2: 72 percent / BF₃*SMe₂ / CH₂Cl₂ / 5 h / 20 °C

With hydrogenchloride; sodium hydroxide; sodium azide; dihydrogen peroxide; sodium hydride; trifluoroacetic acid; copper(l) iodide; L-proline; In diethyl ether; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm070079j

Reference yield:

: 943439-52-9
2-(4-bromo-phenyl)-6-methoxy-benzo[b]thiophene

: 943439-58-5
C₂₇H₂₈SO₃N₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 95 percent / N-bromoacetamide / CH₂Cl₂ / 2 h / 20 °C

2.1: 65 percent / TFA; aq. H₂O₂ / CH₂Cl₂ / 2 h / 20 °C

3.1: NaH / dimethylformamide / 0.33 h

3.2: 94 percent / dimethylformamide / 1 h / 20 °C

4.1: HCl / CH₂Cl₂; diethyl ether / 1 h

4.2: 85 percent / TMSCl; Ph₃P / tetrahydrofuran / 8 h / Heating

5.1: 74 percent / NaN₃; NaOH / CuI; L-proline / dimethylsulfoxide; ethanol / 10 h / 110 °C

6.1: HCl / CH₂Cl₂; diethyl ether / 0.5 h / 20 °C

6.2: 72 percent / BF₃*SMe₂ / CH₂Cl₂ / 5 h / 20 °C

With hydrogenchloride; sodium hydroxide; sodium azide; dihydrogen peroxide; sodium hydride; trifluoroacetic acid; N-bromoacetamide; copper(l) iodide; L-proline; In diethyl ether; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm070079j