(1R)-10-(phenylsulfonyl)isobornyl 3-oxo-2-(triphenylphosphoranylidene)butanoate

Base Information

Chemical Name:(1R)-10-(phenylsulfonyl)isobornyl 3-oxo-2-(triphenylphosphoranylidene)butanoate
CAS No.:607732-32-1
Molecular Formula:C₃₈H₃₉O₅PS
Molecular Weight:638.764
Hs Code.:

Synonyms:(1R)-10-(phenylsulfonyl)isobornyl 3-oxo-2-(triphenylphosphoranylidene)butanoate

Suppliers and Price of (1R)-10-(phenylsulfonyl)isobornyl 3-oxo-2-(triphenylphosphoranylidene)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R)-10-(phenylsulfonyl)isobornyl 3-oxo-2-(triphenylphosphoranylidene)butanoate

Chemical Property:

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Technology Process of (1R)-10-(phenylsulfonyl)isobornyl 3-oxo-2-(triphenylphosphoranylidene)butanoate

There total 4 articles about (1R)-10-(phenylsulfonyl)isobornyl 3-oxo-2-(triphenylphosphoranylidene)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 75-36-5
acetyl chloride

: 741257-92-1
(1R)-(+)-10-(phenylsulfonyl)isobornyl (triphenylphosphoranylidene)acetate

: 607732-32-1
(1R)-10-(phenylsulfonyl)isobornyl 3-oxo-2-(triphenylphosphoranylidene)butanoate

Guidance literature:: With benzenesulfonamide;
DOI:10.1002/ejoc.200400413

Reference yield: 63.0%

: 75-36-5
acetyl chloride

: 741257-92-1
(1R)-(+)-10-(phenylsulfonyl)isobornyl (triphenylphosphoranylidene)acetate

: 607732-31-0
(1R)-(+)-10-(phenylsulfonyl)isobornyl buta-2,3-dienoate

: 607732-32-1
(1R)-10-(phenylsulfonyl)isobornyl 3-oxo-2-(triphenylphosphoranylidene)butanoate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1002/ejoc.200400413

Reference yield:

: (1R)-(-)-10-(phenylsulfonyl)isoborneol

: 607732-32-1
(1R)-10-(phenylsulfonyl)isobornyl 3-oxo-2-(triphenylphosphoranylidene)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / CH₂Cl₂ / 12 h / 20 °C

2: 87 percent / toluene / 12 h / Heating

3: 3 percent / Et₃N / tetrahydrofuran / 12 h / 20 °C

With triethylamine; In tetrahydrofuran; dichloromethane; toluene; 2: Wittig reaction / 3: Wittig reaction;
DOI:10.1002/ejoc.200400413