2-<2-(3,4-dimethoxyphenyl)-3,4-dimethoxyphenyl>-3,4,4-trimethyl-2-oxazolinium iodide

Base Information

Chemical Name:2-<2-(3,4-dimethoxyphenyl)-3,4-dimethoxyphenyl>-3,4,4-trimethyl-2-oxazolinium iodide
CAS No.:85010-21-5
Molecular Formula:C₂₂H₂₈NO₅*I
Molecular Weight:513.373
Hs Code.:

Synonyms:2-<2-(3,4-dimethoxyphenyl)-3,4-dimethoxyphenyl>-3,4,4-trimethyl-2-oxazolinium iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-<2-(3,4-dimethoxyphenyl)-3,4-dimethoxyphenyl>-3,4,4-trimethyl-2-oxazolinium iodide

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Technology Process of 2-<2-(3,4-dimethoxyphenyl)-3,4-dimethoxyphenyl>-3,4,4-trimethyl-2-oxazolinium iodide

There total 5 articles about 2-<2-(3,4-dimethoxyphenyl)-3,4-dimethoxyphenyl>-3,4,4-trimethyl-2-oxazolinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 85010-20-4
2-<2-(3,4-dimethoxyphenyl)-3,4-dimethoxyphenyl>-4,4-dimethyl-2-oxazoline

: 74-88-4
methyl iodide

: 85010-21-5
2-<2-(3,4-dimethoxyphenyl)-3,4-dimethoxyphenyl>-3,4,4-trimethyl-2-oxazolinium iodide

Guidance literature:: In nitromethane; at 70 ℃;

Reference yield:

: 573-11-5
2,3,4-Trimethoxy-benzoic acid

: 85010-21-5
2-<2-(3,4-dimethoxyphenyl)-3,4-dimethoxyphenyl>-3,4,4-trimethyl-2-oxazolinium iodide

Guidance literature:: Multi-step reaction with 5 steps

1: SOCl₂ / 24 h / Ambient temperature

2: CH₂Cl₂ / 1 h / 0 °C

3: 93 percent / SOCl₂

4: 92 percent / tetrahydrofuran / 1.) reflux, 10 min, 2.) room temperature, 20 h

5: 96 percent / nitromethane / 70 °C

With thionyl chloride; In tetrahydrofuran; nitromethane; dichloromethane;

Reference yield:

: 7169-07-5
3,4,5-(trimethoxy)benzoyl chloride

: 85010-21-5
2-<2-(3,4-dimethoxyphenyl)-3,4-dimethoxyphenyl>-3,4,4-trimethyl-2-oxazolinium iodide

Guidance literature:: Multi-step reaction with 4 steps

1: CH₂Cl₂ / 1 h / 0 °C

2: 93 percent / SOCl₂

3: 92 percent / tetrahydrofuran / 1.) reflux, 10 min, 2.) room temperature, 20 h

4: 96 percent / nitromethane / 70 °C

With thionyl chloride; In tetrahydrofuran; nitromethane; dichloromethane;