((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O

Base Information

Chemical Name:((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O
CAS No.:90030-13-0
Molecular Formula:C₃₄H₃₄N₂O₆
Molecular Weight:566.654
Hs Code.:

((C<sub>2</sub>H<sub>4</sub>O)2C<sub>6</sub>H<sub>4</sub>)NC<sub>5</sub>H<sub>2</sub>C<sub>2</sub>H<sub>2</sub>C<sub>5</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>4</sub>(C<sub>2</sub>H<sub>4</sub>O)2)OC<sub>2</sub>H<sub>4</sub>O

Synonyms:((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O

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Chemical Property of ((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O

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Technology Process of ((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O

There total 1 articles about ((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89333-97-1
2,9-bis-(4-methoxy-phenyl)-1,10-phenanthroline

: 90030-13-0
((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O

Guidance literature:: Multi-step reaction with 2 steps

1: chlorure de pyridinium / 200 °C

2: 45 percent / Cs₂CO₃ / dimethylformamide / 50 °C

With pyridine hydrochloride; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)94049-8

Reference yield: 100.0%

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: 90030-13-0
((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O

: 4-(9-{4-[5''-(3-{4-[Tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-propyl)-[2,2';6',2'']terpyridin-5-yl]-butyl}-[1,10]phenanthrolin-2-yl)-phenol

: 190366-49-5
Cu(C₃₄H₃₄N₂O₆)(C₇₇H₇₇N₅O₂)⁽¹⁺⁾

Guidance literature:: In dichloromethane; acetonitrile; Ar atmosphere; addn. of soln. of Cu-complex (in MeCN) to soln. of macrocycle (in CH2Cl2), stirring (room temp., 20 min), addn. of soln. of 2nd.ligand (in CH2Cl2), stirring (room temp., 14 h); evapn.;
DOI:10.1021/ja984051w

Reference yield: 99.0%

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: 89333-97-1
2,9-bis-(4-methoxy-phenyl)-1,10-phenanthroline

: 90030-13-0
((C₂H₄O)2C₆H₄)NC₅H₂C₂H₂C₅H₂N(C₆H₄(C₂H₄O)2)OC₂H₄O

: (Cu(N₂C₂₄H₁₄(O(CH₂CH₂O)2CH₂)2)(N₂C₁₂H₆(C₆H₄OCH₃)2))⁽¹⁺⁾*PF₆^(1-)=(Cu(N₂C₂₄H₁₄(O(CH₂CH₂O)2CH₂)2)(N₂C₁₂H₆(C₆H₄OCH₃)2))PF₆

Guidance literature:: In dichloromethane; acetonitrile; (Ar) soln. Cu complex in MeCN was added to soln. macrocycle in CH2Cl2, soln. diimine in CH2Cl2 was added and stirred for 2 h at room temp.; solvents were removed in vacuo, residue was dissolved in MeCN, filtered and evapd.;
DOI:10.1139/V10-093