3-(benzyloxycarbonylamino)-N-[(1S)-2-hydroxy-1-(1H-imidazol-5-yl-methyl)ethyl]propanamide

Base Information

Chemical Name:3-(benzyloxycarbonylamino)-N-[(1S)-2-hydroxy-1-(1H-imidazol-5-yl-methyl)ethyl]propanamide
CAS No.:1313206-50-6
Molecular Formula:C₁₇H₂₂N₄O₄
Molecular Weight:346.386
Hs Code.:

Synonyms:3-(benzyloxycarbonylamino)-N-[(1S)-2-hydroxy-1-(1H-imidazol-5-yl-methyl)ethyl]propanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(benzyloxycarbonylamino)-N-[(1S)-2-hydroxy-1-(1H-imidazol-5-yl-methyl)ethyl]propanamide

Chemical Property:

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Technology Process of 3-(benzyloxycarbonylamino)-N-[(1S)-2-hydroxy-1-(1H-imidazol-5-yl-methyl)ethyl]propanamide

There total 4 articles about 3-(benzyloxycarbonylamino)-N-[(1S)-2-hydroxy-1-(1H-imidazol-5-yl-methyl)ethyl]propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1318262-66-6
3-(benzyloxycarbonylamino)propionyl-L-histidine ethyl ester

: 1313206-50-6
3-(benzyloxycarbonylamino)-N-[(1S)-2-hydroxy-1-(1H-imidazol-5-yl-methyl)ethyl]propanamide

Guidance literature:: With sodium tetrahydroborate; water; lithium chloride; In methanol; at 20 - 25 ℃; for 15.5h; Inert atmosphere;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1313206-50-6
3-(benzyloxycarbonylamino)-N-[(1S)-2-hydroxy-1-(1H-imidazol-5-yl-methyl)ethyl]propanamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / water; acetone / 16 h / 0 - 25 °C / pH 12 - 13

1.2: pH 2 - 2.5

2.1: hydrogenchloride / 15 h / 20 - 30 °C / Inert atmosphere

2.2: 0.5 h / 0 - 25 °C / pH 7 - 7.5 / Inert atmosphere

3.1: water; lithium chloride; sodium tetrahydroborate / methanol / 15.5 h / 20 - 25 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; water; lithium chloride; sodium hydroxide; In methanol; water; acetone;

Reference yield:

: 305-84-0
Carnosine

: 1313206-50-6
3-(benzyloxycarbonylamino)-N-[(1S)-2-hydroxy-1-(1H-imidazol-5-yl-methyl)ethyl]propanamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / water; acetone / 16 h / 0 - 25 °C / pH 12 - 13

1.2: pH 2 - 2.5

2.1: hydrogenchloride / 15 h / 20 - 30 °C / Inert atmosphere

2.2: 0.5 h / 0 - 25 °C / pH 7 - 7.5 / Inert atmosphere

3.1: water; lithium chloride; sodium tetrahydroborate / methanol / 15.5 h / 20 - 25 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; water; lithium chloride; sodium hydroxide; In methanol; water; acetone;