1-<4-tert-butyl-3'-(2-methoxyethoxymethyl)benzhydryl>-4-benzylpiperazine

Base Information

Chemical Name:1-<4-tert-butyl-3'-(2-methoxyethoxymethyl)benzhydryl>-4-benzylpiperazine
CAS No.:219502-63-3
Molecular Formula:C₃₂H₄₂N₂O₃
Molecular Weight:502.697
Hs Code.:

Synonyms:1-<4-tert-butyl-3'-(2-methoxyethoxymethyl)benzhydryl>-4-benzylpiperazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<4-tert-butyl-3'-(2-methoxyethoxymethyl)benzhydryl>-4-benzylpiperazine

Chemical Property:

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Technology Process of 1-<4-tert-butyl-3'-(2-methoxyethoxymethyl)benzhydryl>-4-benzylpiperazine

There total 4 articles about 1-<4-tert-butyl-3'-(2-methoxyethoxymethyl)benzhydryl>-4-benzylpiperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 2759-28-6
1-phenylmethylpiperazine

: 219502-62-2
4-tert-butyl-3'-(2-methoxyethoxymethyl)benzhydryl chloride

: 219502-63-3
1-<4-tert-butyl-3'-(2-methoxyethoxymethyl)benzhydryl>-4-benzylpiperazine

Guidance literature:: With potassium carbonate; In acetonitrile; for 2h; Heating;
DOI:10.1021/jm980374r

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 219502-63-3
1-<4-tert-butyl-3'-(2-methoxyethoxymethyl)benzhydryl>-4-benzylpiperazine

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / DIEA / CH₂Cl₂ / 3 h / Ambient temperature

2: 80 percent / tetrahydrofuran / 0 - 20 °C

3: 70 percent / PPh₃, CCl₄ / 3 h / Heating

4: 70 percent / K₂CO₃ / acetonitrile / 2 h / Heating

With tetrachloromethane; potassium carbonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jm980374r

Reference yield:

: 139461-72-6
(3-methoxyethoxymethyloxy)benzaldehyde

: 219502-63-3
1-<4-tert-butyl-3'-(2-methoxyethoxymethyl)benzhydryl>-4-benzylpiperazine

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / tetrahydrofuran / 0 - 20 °C

2: 70 percent / PPh₃, CCl₄ / 3 h / Heating

3: 70 percent / K₂CO₃ / acetonitrile / 2 h / Heating

With tetrachloromethane; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jm980374r