2,2,5-Trimethyl-3-dichloroacetyl-1,3-oxazolidine

Base Information

• Chemical Name: 2,2,5-Trimethyl-3-dichloroacetyl-1,3-oxazolidine
• CAS No.: 52836-31-4
• Molecular Formula: C8H13 Cl2 N O2
• Molecular Weight: 226.103
• Hs Code.: 2934999090
• European Community (EC) Number: 258-214-7
• UNII: JLY7K2SJEK
• DSSTox Substance ID: DTXSID5028031
• Nikkaji Number: J10.893F
• Wikidata: Q27281571
• ChEMBL ID: CHEMBL2269057
• Mol file: 52836-31-4.mol

Synonyms:3-(dichloroacetyl)-2,2,5-trimethyl-1,3-oxazolidine;R 29148;R-29148

Chemical Property of 2,2,5-Trimethyl-3-dichloroacetyl-1,3-oxazolidine

Chemical Property:

• Vapor Pressure: 0.00196mmHg at 25°C
• Boiling Point: 291.4 °C at 760 mmHg
• Flash Point: 130 °C
• PSA: 29.54000
• Density: 1.231 g/cm³
• LogP: 1.71140
• Storage Temp.: Refrigerator, under inert atmosphere
• Solubility.: Chloroform (Slightly), Methanol (Slightly)
• XLogP3: 1.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 225.0323340
• Heavy Atom Count: 13
• Complexity: 218

Purity/Quality:

99%, ^*data from raw suppliers

2,2-Dichloro-1-(2,2,5-trimethyloxazolidin-3-yl)ethanone 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1CN(C(O1)(C)C)C(=O)C(Cl)Cl
• Uses: 3-(Dichloroacetyl)-2,2,5-trimethyloxazolidine is used in the synthesis of?herbicidal compositions containing methiozolin.

Technology Process of 2,2,5-Trimethyl-3-dichloroacetyl-1,3-oxazolidine

There total 2 articles about 2,2,5-Trimethyl-3-dichloroacetyl-1,3-oxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dichloroacethyl chloride (79-36-7) + 2,2,5-trimethyl-2,3,4,5-tetrahydroisoxazole (52837-54-4) → R-29148 (52836-31-4)

Guidance literature:

With triethylamine; In benzene;

Reference yield:

→ R-29148 (52836-31-4)

Guidance literature:

2,2,2-Trimethyl-oxazolidin,Dichloressigsaeurechlorid;

upstream raw materials:

dichloroacethyl chloride

2,2,5-trimethyl-2,3,4,5-tetrahydroisoxazole

Refernces

• 1、 -. "Herbicide antidotes as safeners for reducing phytotoxicity resulting from synergistic interaction between herbicides and other pesticides". . . Retrieved 2008/06/13.
• 2、 -. "N-acylation of oxazolidines". . . Retrieved 2008/06/13.