(Z)-(4-((4-((1-(4-fluorobenzyl)-3-methyl-2,5-dioxoimidazolidin-4-ylidene)methyl)phenoxy)methyl)phenyl)boronic acid

Base Information

Chemical Name:(Z)-(4-((4-((1-(4-fluorobenzyl)-3-methyl-2,5-dioxoimidazolidin-4-ylidene)methyl)phenoxy)methyl)phenyl)boronic acid
CAS No.:1312201-49-2
Molecular Formula:C₂₅H₂₂BFN₂O₅
Molecular Weight:460.269
Hs Code.:

Synonyms:(Z)-(4-((4-((1-(4-fluorobenzyl)-3-methyl-2,5-dioxoimidazolidin-4-ylidene)methyl)phenoxy)methyl)phenyl)boronic acid

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Chemical Property of (Z)-(4-((4-((1-(4-fluorobenzyl)-3-methyl-2,5-dioxoimidazolidin-4-ylidene)methyl)phenoxy)methyl)phenyl)boronic acid

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Technology Process of (Z)-(4-((4-((1-(4-fluorobenzyl)-3-methyl-2,5-dioxoimidazolidin-4-ylidene)methyl)phenoxy)methyl)phenyl)boronic acid

There total 8 articles about (Z)-(4-((4-((1-(4-fluorobenzyl)-3-methyl-2,5-dioxoimidazolidin-4-ylidene)methyl)phenoxy)methyl)phenyl)boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: (Z)-(4-((4-((1-(4-fluorobenzyl)-2,5-dioxoimidazolidin-4-ylidene)methyl)phenoxy)methyl)phenyl)boronic acid

: 74-88-4
methyl iodide

: 1312201-49-2
(Z)-(4-((4-((1-(4-fluorobenzyl)-3-methyl-2,5-dioxoimidazolidin-4-ylidene)methyl)phenoxy)methyl)phenyl)boronic acid

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 4h;
DOI:10.1021/jm200310q

Reference yield: 68.0%

: 1229652-28-1
(4-((4-formylphenoxy)methyl)phenyl)boronic acid

: 1312201-47-0
3-(4-fluorobenzyl)-1-methylimidazolidine-2,4-dione

: 1312201-64-1
(E)-(4-((4-((1-(4-fluorobenzyl)-3-methyl-2,5-dioxoimidazolidin-4-ylidene)methyl)phenoxy)methyl)phenyl)boronic acid

: 1312201-49-2
(Z)-(4-((4-((1-(4-fluorobenzyl)-3-methyl-2,5-dioxoimidazolidin-4-ylidene)methyl)phenoxy)methyl)phenyl)boronic acid

Guidance literature:: With piperidine; In ethanol; for 22h; Reflux;
DOI:10.1021/jm200310q

Reference yield:

: 1312201-10-7
4-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)oxy)benzaldehyde

: 1312201-64-1
(E)-(4-((4-((1-(4-fluorobenzyl)-3-methyl-2,5-dioxoimidazolidin-4-ylidene)methyl)phenoxy)methyl)phenyl)boronic acid

: 1312201-49-2
(Z)-(4-((4-((1-(4-fluorobenzyl)-3-methyl-2,5-dioxoimidazolidin-4-ylidene)methyl)phenoxy)methyl)phenyl)boronic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium periodate / tetrahydrofuran; water / 0.5 h

1.2: 4 h

2.1: piperidine / ethanol / 22 h / Reflux

With piperidine; sodium periodate; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jm200310q