C₆₄H₁₁₈O₈Si₄

Base Information

Chemical Name:C₆₄H₁₁₈O₈Si₄
CAS No.:208984-65-0
Molecular Formula:C₆₄H₁₁₈O₈Si₄
Molecular Weight:1127.98
Hs Code.:

C<sub>64</sub>H<sub>118</sub>O<sub>8</sub>Si<sub>4</sub>

Synonyms:C₆₄H₁₁₈O₈Si₄

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Chemical Property of C₆₄H₁₁₈O₈Si₄

Chemical Property:

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Technology Process of C₆₄H₁₁₈O₈Si₄

There total 39 articles about C₆₄H₁₁₈O₈Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 208984-65-0
C₆₄H₁₁₈O₈Si₄

Guidance literature:: Multi-step reaction with 19 steps

1: 100 percent / 2,6-lutidine / CH₂Cl₂

2: 92 percent / H₂ / Pd(OH)2/C / ethanol

3: 98 percent / SO₃*pyridine, Et₃N / dimethylsulfoxide

4: 79 percent / ZnCl₂ / diethyl ether

5: 91 percent / DIBAL / tetrahydrofuran

6: 99 percent / TsOH*H₂O / methanol

7: 1.) t-BuLi, HMPA / 1.) THF, 2.) THF

8: 80 percent / PhI(CF₃CO₃)2 / methanol; H₂O

9: 97 percent / Me₄NBH(OAc)3

10: 87 percent / TsOH*H₂O / benzene

11: 98 percent / 2,6-lutidine / CH₂Cl₂

12: 100 percent / H₂ / Pd/C / ethanol; ethyl acetate

13: 83 percent / MgBr₂ / diethyl ether

14: 86 percent / (COCl)2, DMSO

15: 1.) NaHMDS / 1.) THF, 2.) THF

16: 88 percent / DIBAL / CH₂Cl₂

17: 70 percent / t-BuLi, Ti(O-i-Pr)4, MeI / tetrahydrofuran

18: HgCl₂ / acetonitrile; tetrahydrofuran

19: DMSO, Ac₂O

With 2,6-dimethylpyridine; titanium(IV) isopropylate; N,N,N,N,N,N-hexamethylphosphoric triamide; oxalyl dichloride; pyridine-SO₃ complex; hydrogen; tert.-butyl lithium; sodium hexamethyldisilazane; acetic anhydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; mercury dichloride; magnesium bromide; zinc(II) chloride; tetramethylammonium triacetoxyborohydride; methyl iodide; palladium dihydroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; acetonitrile; benzene;
DOI:10.1021/ja00153a030

Reference yield:

: 172269-36-2
(S)-4-benzyl-3-{(2S,3R,4R)-3-hydroxy-5-[(4methoxybenzyl)oxy]-2,4-dimethylpentanoyl}oxazolidin-2-one

: 208984-65-0
C₆₄H₁₁₈O₈Si₄

Guidance literature:: Multi-step reaction with 20 steps

1: 89 percent / AlMe₃ / tetrahydrofuran

2: 100 percent / 2,6-lutidine / CH₂Cl₂

3: 92 percent / H₂ / Pd(OH)2/C / ethanol

4: 98 percent / SO₃*pyridine, Et₃N / dimethylsulfoxide

5: 79 percent / ZnCl₂ / diethyl ether

6: 91 percent / DIBAL / tetrahydrofuran

7: 99 percent / TsOH*H₂O / methanol

8: 1.) t-BuLi, HMPA / 1.) THF, 2.) THF

9: 80 percent / PhI(CF₃CO₃)2 / methanol; H₂O

10: 97 percent / Me₄NBH(OAc)3

11: 87 percent / TsOH*H₂O / benzene

12: 98 percent / 2,6-lutidine / CH₂Cl₂

13: 100 percent / H₂ / Pd/C / ethanol; ethyl acetate

14: 83 percent / MgBr₂ / diethyl ether

15: 86 percent / (COCl)2, DMSO

16: 1.) NaHMDS / 1.) THF, 2.) THF

17: 88 percent / DIBAL / CH₂Cl₂

18: 70 percent / t-BuLi, Ti(O-i-Pr)4, MeI / tetrahydrofuran

19: HgCl₂ / acetonitrile; tetrahydrofuran

20: DMSO, Ac₂O

With 2,6-dimethylpyridine; titanium(IV) isopropylate; N,N,N,N,N,N-hexamethylphosphoric triamide; oxalyl dichloride; pyridine-SO₃ complex; hydrogen; trimethylaluminum; tert.-butyl lithium; sodium hexamethyldisilazane; acetic anhydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; mercury dichloride; magnesium bromide; zinc(II) chloride; tetramethylammonium triacetoxyborohydride; methyl iodide; palladium dihydroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; acetonitrile; benzene;
DOI:10.1021/ja00153a030

Reference yield:

: 172269-19-1
(2S,3R,4R)-3-Hydroxy-5-(4-methoxy-benzyloxy)-2,4-dimethyl-pentanoic acid methoxy-methyl-amide

: 208984-65-0
C₆₄H₁₁₈O₈Si₄

Guidance literature:: Multi-step reaction with 19 steps

1: 100 percent / 2,6-lutidine / CH₂Cl₂

2: 92 percent / H₂ / Pd(OH)2/C / ethanol

3: 98 percent / SO₃*pyridine, Et₃N / dimethylsulfoxide

4: 79 percent / ZnCl₂ / diethyl ether

5: 91 percent / DIBAL / tetrahydrofuran

6: 99 percent / TsOH*H₂O / methanol

7: 1.) t-BuLi, HMPA / 1.) THF, 2.) THF

8: 80 percent / PhI(CF₃CO₃)2 / methanol; H₂O

9: 97 percent / Me₄NBH(OAc)3

10: 87 percent / TsOH*H₂O / benzene

11: 98 percent / 2,6-lutidine / CH₂Cl₂

12: 100 percent / H₂ / Pd/C / ethanol; ethyl acetate

13: 83 percent / MgBr₂ / diethyl ether

14: 86 percent / (COCl)2, DMSO

15: 1.) NaHMDS / 1.) THF, 2.) THF

16: 88 percent / DIBAL / CH₂Cl₂

17: 70 percent / t-BuLi, Ti(O-i-Pr)4, MeI / tetrahydrofuran

18: HgCl₂ / acetonitrile; tetrahydrofuran

19: DMSO, Ac₂O

With 2,6-dimethylpyridine; titanium(IV) isopropylate; N,N,N,N,N,N-hexamethylphosphoric triamide; oxalyl dichloride; pyridine-SO₃ complex; hydrogen; tert.-butyl lithium; sodium hexamethyldisilazane; acetic anhydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; mercury dichloride; magnesium bromide; zinc(II) chloride; tetramethylammonium triacetoxyborohydride; methyl iodide; palladium dihydroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; acetonitrile; benzene;
DOI:10.1021/ja00153a030