methyl 2-[{2-(5-(benzyloxy)-4,4-dimethylpent-1-en-2-yl)phenyl}(methoxycarbonyl)amino]acetate

Base Information

Chemical Name:methyl 2-[{2-(5-(benzyloxy)-4,4-dimethylpent-1-en-2-yl)phenyl}(methoxycarbonyl)amino]acetate
CAS No.:1402615-67-1
Molecular Formula:C₂₅H₃₁NO₅
Molecular Weight:425.525
Hs Code.:

Synonyms:methyl 2-[{2-(5-(benzyloxy)-4,4-dimethylpent-1-en-2-yl)phenyl}(methoxycarbonyl)amino]acetate

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Chemical Property of methyl 2-[{2-(5-(benzyloxy)-4,4-dimethylpent-1-en-2-yl)phenyl}(methoxycarbonyl)amino]acetate

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Technology Process of methyl 2-[{2-(5-(benzyloxy)-4,4-dimethylpent-1-en-2-yl)phenyl}(methoxycarbonyl)amino]acetate

There total 6 articles about methyl 2-[{2-(5-(benzyloxy)-4,4-dimethylpent-1-en-2-yl)phenyl}(methoxycarbonyl)amino]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1402615-98-8
C₂₂H₂₇NO₃

: 96-32-2
bromoacetic acid methyl ester

: 1402615-67-1
methyl 2-[{2-(5-(benzyloxy)-4,4-dimethylpent-1-en-2-yl)phenyl}(methoxycarbonyl)amino]acetate

Guidance literature:: C₂₂H₂₇NO₃; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere;

bromoacetic acid methyl ester; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1021/jo301817w DOI:10.1021/jo301817w

Reference yield:

: 1402615-56-8
2-[5-(benzyloxy)-4,4-dimethylpent-1-en-2-yl]aniline

: 1402615-67-1
methyl 2-[{2-(5-(benzyloxy)-4,4-dimethylpent-1-en-2-yl)phenyl}(methoxycarbonyl)amino]acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / water; tetrahydrofuran / 3 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C

With sodium hydride; potassium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/jo301817w DOI:10.1021/jo301817w

Reference yield:

: 1402615-50-2
[(2,2-dimethylpenta-3,4-dienyloxy)methyl]benzene

: 1402615-67-1
methyl 2-[{2-(5-(benzyloxy)-4,4-dimethylpent-1-en-2-yl)phenyl}(methoxycarbonyl)amino]acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; 2BF₄^(1-)*C₇₂H₆₂O₂P₄Pt₂⁽⁴⁺⁾ / water; 1,4-dioxane / 100 °C / Inert atmosphere

2.1: potassium carbonate / water; tetrahydrofuran / 3 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C

With 2BF₄^(1-)*C₇₂H₆₂O₂P₄Pt₂⁽⁴⁺⁾; sodium hydride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo301817w DOI:10.1021/jo301817w