2,2'-(1-phenylprop-2-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Base Information

Chemical Name:2,2'-(1-phenylprop-2-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)
CAS No.:206858-39-1
Molecular Formula:C₂₁H₃₂B₂O₄
Molecular Weight:370.105
Hs Code.:

Synonyms:2,2'-(1-phenylprop-2-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Chemical Property of 2,2'-(1-phenylprop-2-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Technology Process of 2,2'-(1-phenylprop-2-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

There total 1 articles about 2,2'-(1-phenylprop-2-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2327-99-3
1-phenylpropadiene

: 73183-34-3
bis(pinacol)diborane

: 206858-39-1
2,2'-(1-phenylprop-2-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tricyclohexylphosphine; In toluene; at 22 ℃;
DOI:10.1021/ol052312i

Reference yield:

: 206858-39-1
2,2'-(1-phenylprop-2-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: C₂₇H₃₈B₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 9 h / 20 °C

2: Cs₂CO₃; H₂O / toluene / 12 h / 80 °C

With water; caesium carbonate; In toluene; 2: Suzuki-Miyaura cross-coupling;
DOI:10.1021/ol0616891

Reference yield:

: 206858-39-1
2,2'-(1-phenylprop-2-ene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 5381-80-6,5381-84-0,5565-57-1,130609-32-4,130609-33-5
rac-(1R,2R)-1,3-diphenylpropane-1,2-diol

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 9 h / 20 °C

2: Cs₂CO₃; H₂O / toluene / 12 h / 80 °C

3: H₂O₂; NaOH / H₂O; tetrahydrofuran; toluene / 0 - 20 °C

With sodium hydroxide; water; dihydrogen peroxide; caesium carbonate; In tetrahydrofuran; water; toluene; 2: Suzuki-Miyaura cross-coupling;
DOI:10.1021/ol0616891