5R-(2,4,6-trifluorophenyl)-5,6-dihydro-N,N-bis[(4-methoxyphenyl)methyl]-2,5-dimethyl-2H-1,2,4-thiadiazin-3-amine-1,1-dioxide

Base Information

Chemical Name:5R-(2,4,6-trifluorophenyl)-5,6-dihydro-N,N-bis[(4-methoxyphenyl)methyl]-2,5-dimethyl-2H-1,2,4-thiadiazin-3-amine-1,1-dioxide
CAS No.:1286794-47-5
Molecular Formula:C₂₇H₂₈F₃N₃O₄S
Molecular Weight:547.598
Hs Code.:

Synonyms:5R-(2,4,6-trifluorophenyl)-5,6-dihydro-N,N-bis[(4-methoxyphenyl)methyl]-2,5-dimethyl-2H-1,2,4-thiadiazin-3-amine-1,1-dioxide

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Chemical Property of 5R-(2,4,6-trifluorophenyl)-5,6-dihydro-N,N-bis[(4-methoxyphenyl)methyl]-2,5-dimethyl-2H-1,2,4-thiadiazin-3-amine-1,1-dioxide

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Technology Process of 5R-(2,4,6-trifluorophenyl)-5,6-dihydro-N,N-bis[(4-methoxyphenyl)methyl]-2,5-dimethyl-2H-1,2,4-thiadiazin-3-amine-1,1-dioxide

There total 1 articles about 5R-(2,4,6-trifluorophenyl)-5,6-dihydro-N,N-bis[(4-methoxyphenyl)methyl]-2,5-dimethyl-2H-1,2,4-thiadiazin-3-amine-1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1286794-47-5
5R-(2,4,6-trifluorophenyl)-5,6-dihydro-N,N-bis[(4-methoxyphenyl)methyl]-2,5-dimethyl-2H-1,2,4-thiadiazin-3-amine-1,1-dioxide

Guidance literature:

Reference yield: 52.0%

: 402-43-7
p-trifluoromethylphenyl bromide

: 1286794-47-5
5R-(2,4,6-trifluorophenyl)-5,6-dihydro-N,N-bis[(4-methoxyphenyl)methyl]-2,5-dimethyl-2H-1,2,4-thiadiazin-3-amine-1,1-dioxide

: 1286794-21-5
6(R)-[4-(trifluoromethyl)phenyl]-5R-(2,4,6-trifluorophenyl)-5,6-dihydro-N,N-bis[(4-methoxyphenyl)methyl]-2,5-dimethyl-2H-l,2,4-thiadiazin-3-amine-1,1-dioxide

Guidance literature:: 5R-(2,4,6-trifluorophenyl)-5,6-dihydro-N,N-bis[(4-methoxyphenyl)methyl]-2,5-dimethyl-2H-1,2,4-thiadiazin-3-amine-1,1-dioxide; With sodium hexamethyldisilazane; In 1,4-dioxane; at 20 ℃; for 0.5h;

With zinc(II) chloride; In 1,4-dioxane; at 20 ℃; for 0.5h;

p-trifluoromethylphenyl bromide; (2’,4’,6’-triisopropyl-[1,1’-biphenyl]-2-yl)-diphenylphosphine; palladium diacetate; In 1,4-dioxane; at 100 ℃; for 3h; Inert atmosphere;

Reference yield: 28.0%

: 1286794-47-5
5R-(2,4,6-trifluorophenyl)-5,6-dihydro-N,N-bis[(4-methoxyphenyl)methyl]-2,5-dimethyl-2H-1,2,4-thiadiazin-3-amine-1,1-dioxide

: 69045-82-5
2-fluoro-5-(trifluoromethyl)pyridine

: 1286794-22-6
6(R)-[5-(trifluoromethyl)-2-pyridyl]-5R-(2,4,6-trifluorophenyl)-5,6-dihydro-N,N-bis[(4-methoxyphenyl)methyl]-2,5-dimethyl-2H-1,2,4-thiadiazin-3-amine-1,1-dioxide

Guidance literature:: 5R-(2,4,6-trifluorophenyl)-5,6-dihydro-N,N-bis[(4-methoxyphenyl)methyl]-2,5-dimethyl-2H-1,2,4-thiadiazin-3-amine-1,1-dioxide; 2-fluoro-5-(trifluoromethyl)pyridine; With zinc(II) chloride; lithium hexamethyldisilazane; In tetrahydrofuran; for 1h;

With sodium hexamethyldisilazane; In tetrahydrofuran; for 3h;

With lithium hexamethyldisilazane; In tetrahydrofuran; toluene; for 2h;