9-(2-benzyloxy-ethyl)-2-methyl-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid diethylamide

Base Information

Chemical Name:9-(2-benzyloxy-ethyl)-2-methyl-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid diethylamide
CAS No.:1246454-05-6
Molecular Formula:C₂₇H₃₄N₂O₂
Molecular Weight:418.579
Hs Code.:

Synonyms:9-(2-benzyloxy-ethyl)-2-methyl-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid diethylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-(2-benzyloxy-ethyl)-2-methyl-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid diethylamide

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Technology Process of 9-(2-benzyloxy-ethyl)-2-methyl-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid diethylamide

There total 5 articles about 9-(2-benzyloxy-ethyl)-2-methyl-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid diethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 1246454-04-5
3-bromo-2-hydroxy-5-methyl-cyclohex-1-enecarboxylic acid diethylamide

: 71126-63-1
N-[2-(phenylmethoxy)ethyl]aniline

: 1246454-05-6
9-(2-benzyloxy-ethyl)-2-methyl-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid diethylamide

Guidance literature:: With zinc(II) chloride; In isopropyl alcohol; at 50 ℃; for 19h; Inert atmosphere; Reflux;

Reference yield:

: 1462-37-9
bromoethyl-2-benzyl ether

: 1246454-05-6
9-(2-benzyloxy-ethyl)-2-methyl-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid diethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 100 °C

2: zinc(II) chloride / isopropyl alcohol / 19 h / 50 °C / Inert atmosphere; Reflux

With 2,6-dimethylpyridine; zinc(II) chloride; In N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 6134-75-4
5-methyl-2-oxocyclohexanecarboxylic acid ethyl ester

: 1246454-05-6
9-(2-benzyloxy-ethyl)-2-methyl-2,3,4,9-tetrahydro-1H-carbazole-4-carboxylic acid diethylamide

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / toluene / 96 h / Reflux

2: bromine / diethyl ether / 1.75 h / 0 - 20 °C / Inert atmosphere

3: zinc(II) chloride / isopropyl alcohol / 19 h / 50 °C / Inert atmosphere; Reflux

With dmap; bromine; zinc(II) chloride; In diethyl ether; isopropyl alcohol; toluene;