methyl 6-{4-[(4-chlorophenyl)thio]-1-phenyl-1H-pyrazol-3-yl}nicotinate

Base Information

Chemical Name:methyl 6-{4-[(4-chlorophenyl)thio]-1-phenyl-1H-pyrazol-3-yl}nicotinate
CAS No.:1199802-65-7
Molecular Formula:C₂₂H₁₆ClN₃O₂S
Molecular Weight:421.907
Hs Code.:

Synonyms:methyl 6-{4-[(4-chlorophenyl)thio]-1-phenyl-1H-pyrazol-3-yl}nicotinate

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Chemical Property of methyl 6-{4-[(4-chlorophenyl)thio]-1-phenyl-1H-pyrazol-3-yl}nicotinate

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Technology Process of methyl 6-{4-[(4-chlorophenyl)thio]-1-phenyl-1H-pyrazol-3-yl}nicotinate

There total 2 articles about methyl 6-{4-[(4-chlorophenyl)thio]-1-phenyl-1H-pyrazol-3-yl}nicotinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7424-91-1
methyl 3,3-dimethoxypropionate

: 1199805-30-5
C₂₀H₁₈ClN₃OS

: 1199802-65-7
methyl 6-{4-[(4-chlorophenyl)thio]-1-phenyl-1H-pyrazol-3-yl}nicotinate

Guidance literature:: With ammonium acetate; In N,N-dimethyl-formamide; at 120 ℃; for 0.333333h; Microwave irradiation;

Reference yield:

: 1199805-03-2
1-(4-[(4-chlorophenyl)thio]-1-phenyl-1H-pyrazol-3-yl)ethanone

: 1199802-65-7
methyl 6-{4-[(4-chlorophenyl)thio]-1-phenyl-1H-pyrazol-3-yl}nicotinate

Guidance literature:: Multi-step reaction with 2 steps

1: 3 h / 120 °C / Microwave irradiation

2: ammonium acetate / N,N-dimethyl-formamide / 0.33 h / 120 °C / Microwave irradiation

With ammonium acetate; In N,N-dimethyl-formamide;

Reference yield:

: 1199802-65-7
methyl 6-{4-[(4-chlorophenyl)thio]-1-phenyl-1H-pyrazol-3-yl}nicotinate

: 75-16-1
methylmagnesium bromide

: 1199802-66-8
C₂₃H₂₀ClN₃OS

Guidance literature:: methyl 6-{4-[(4-chlorophenyl)thio]-1-phenyl-1H-pyrazol-3-yl}nicotinate; methylmagnesium bromide; In tetrahydrofuran; at 20 ℃;

With hydrogenchloride; water; In tetrahydrofuran;