(S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-6-benzyloxycarbonylamino-hexanoylamino]-6-benzyloxycarbonylamino-hexanoylamino}-4-methyl-pentanoic acid 4-nitro-phenyl ester; hydrochloride

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Chemical Name:(S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-6-benzyloxycarbonylamino-hexanoylamino]-6-benzyloxycarbonylamino-hexanoylamino}-4-methyl-pentanoic acid 4-nitro-phenyl ester; hydrochloride
CAS No.:123795-49-3
Molecular Formula:C₄₆H₆₃N₇O₁₁*ClH
Molecular Weight:926.507
Hs Code.:

(S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-6-benzyloxycarbonylamino-hexanoylamino]-6-benzyloxycarbonylamino-hexanoylamino}-4-methyl-pentanoic acid 4-nitro-phenyl ester; hydrochloride

Synonyms:(S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-6-benzyloxycarbonylamino-hexanoylamino]-6-benzyloxycarbonylamino-hexanoylamino}-4-methyl-pentanoic acid 4-nitro-phenyl ester; hydrochloride

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Chemical Property of (S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-6-benzyloxycarbonylamino-hexanoylamino]-6-benzyloxycarbonylamino-hexanoylamino}-4-methyl-pentanoic acid 4-nitro-phenyl ester; hydrochloride

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Technology Process of (S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-6-benzyloxycarbonylamino-hexanoylamino]-6-benzyloxycarbonylamino-hexanoylamino}-4-methyl-pentanoic acid 4-nitro-phenyl ester; hydrochloride

There total 6 articles about (S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-6-benzyloxycarbonylamino-hexanoylamino]-6-benzyloxycarbonylamino-hexanoylamino}-4-methyl-pentanoic acid 4-nitro-phenyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 123795-48-2
(S)-2-((S)-6-Benzyloxycarbonylamino-2-{(S)-6-benzyloxycarbonylamino-2-[(S)-4-methyl-2-(2-nitro-phenylsulfanylamino)-pentanoylamino]-hexanoylamino}-hexanoylamino)-4-methyl-pentanoic acid 4-nitro-phenyl ester

: 123795-49-3
(S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-6-benzyloxycarbonylamino-hexanoylamino]-6-benzyloxycarbonylamino-hexanoylamino}-4-methyl-pentanoic acid 4-nitro-phenyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; chloroform; for 0.25h;

Reference yield:

: 7675-62-9
N^α-2-nitrobenzenesulfenyl-N^ε-benzyloxycarbonyllysine dicyclohexylammonium salt

: 123795-49-3
(S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-6-benzyloxycarbonylamino-hexanoylamino]-6-benzyloxycarbonylamino-hexanoylamino}-4-methyl-pentanoic acid 4-nitro-phenyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 61 percent / DCC / CHCl₃ / 1. -10 deg C, 2 h; 2. room temperature, 2 h

2: 91 percent / HCl / acetone; diethyl ether / 0.25 h

3: 1. N-methylmorpholine, isobutyl chloroformate; 2. N-methylmorpholine / 1. THF, -10 deg C, 15 min; 2. -10 deg C, 1 h, room temperature, 2 h

4: 95 percent / HCl / CHCl₃; diethyl ether / 0.25 h

With 4-methyl-morpholine; hydrogenchloride; dicyclohexyl-carbodiimide; isobutyl chloroformate; In diethyl ether; chloroform; acetone;

Reference yield:

: 7675-50-5
o-nitrobenzenesulphenylleucine dicyclohexylammonium salt

: 123795-49-3
(S)-2-{(S)-2-[(S)-2-((S)-2-Amino-4-methyl-pentanoylamino)-6-benzyloxycarbonylamino-hexanoylamino]-6-benzyloxycarbonylamino-hexanoylamino}-4-methyl-pentanoic acid 4-nitro-phenyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1. N-methylmorpholine, isobutyl chloroformate; 2. N-methylmorpholine / 1. THF, -10 deg C, 15 min; 2. -10 deg C, 1 h, room temperature, 2 h

2: 95 percent / HCl / CHCl₃; diethyl ether / 0.25 h

With 4-methyl-morpholine; hydrogenchloride; isobutyl chloroformate; In diethyl ether; chloroform;