(S)-2-((S)-6-Benzyloxycarbonylamino-2-{(S)-6-benzyloxycarbonylamino-2-[(S)-4-methyl-2-(2-nitro-phenylsulfanylamino)-pentanoylamino]-hexanoylamino}-hexanoylamino)-4-methyl-pentanoic acid 4-nitro-phenyl ester

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Chemical Name:(S)-2-((S)-6-Benzyloxycarbonylamino-2-{(S)-6-benzyloxycarbonylamino-2-[(S)-4-methyl-2-(2-nitro-phenylsulfanylamino)-pentanoylamino]-hexanoylamino}-hexanoylamino)-4-methyl-pentanoic acid 4-nitro-phenyl ester
CAS No.:123795-48-2
Molecular Formula:C₅₂H₆₆N₈O₁₃S
Molecular Weight:1043.21
Hs Code.:

(S)-2-((S)-6-Benzyloxycarbonylamino-2-{(S)-6-benzyloxycarbonylamino-2-[(S)-4-methyl-2-(2-nitro-phenylsulfanylamino)-pentanoylamino]-hexanoylamino}-hexanoylamino)-4-methyl-pentanoic acid 4-nitro-phenyl ester

Synonyms:(S)-2-((S)-6-Benzyloxycarbonylamino-2-{(S)-6-benzyloxycarbonylamino-2-[(S)-4-methyl-2-(2-nitro-phenylsulfanylamino)-pentanoylamino]-hexanoylamino}-hexanoylamino)-4-methyl-pentanoic acid 4-nitro-phenyl ester

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Chemical Property of (S)-2-((S)-6-Benzyloxycarbonylamino-2-{(S)-6-benzyloxycarbonylamino-2-[(S)-4-methyl-2-(2-nitro-phenylsulfanylamino)-pentanoylamino]-hexanoylamino}-hexanoylamino)-4-methyl-pentanoic acid 4-nitro-phenyl ester

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Technology Process of (S)-2-((S)-6-Benzyloxycarbonylamino-2-{(S)-6-benzyloxycarbonylamino-2-[(S)-4-methyl-2-(2-nitro-phenylsulfanylamino)-pentanoylamino]-hexanoylamino}-hexanoylamino)-4-methyl-pentanoic acid 4-nitro-phenyl ester

There total 4 articles about (S)-2-((S)-6-Benzyloxycarbonylamino-2-{(S)-6-benzyloxycarbonylamino-2-[(S)-4-methyl-2-(2-nitro-phenylsulfanylamino)-pentanoylamino]-hexanoylamino}-hexanoylamino)-4-methyl-pentanoic acid 4-nitro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7675-62-9
N^α-2-nitrobenzenesulfenyl-N^ε-benzyloxycarbonyllysine dicyclohexylammonium salt

: 123795-48-2
(S)-2-((S)-6-Benzyloxycarbonylamino-2-{(S)-6-benzyloxycarbonylamino-2-[(S)-4-methyl-2-(2-nitro-phenylsulfanylamino)-pentanoylamino]-hexanoylamino}-hexanoylamino)-4-methyl-pentanoic acid 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / DCC / CHCl₃ / 1. -10 deg C, 2 h; 2. room temperature, 2 h

2: 91 percent / HCl / acetone; diethyl ether / 0.25 h

3: 1. N-methylmorpholine, isobutyl chloroformate; 2. N-methylmorpholine / 1. THF, -10 deg C, 15 min; 2. -10 deg C, 1 h, room temperature, 2 h

With 4-methyl-morpholine; hydrogenchloride; dicyclohexyl-carbodiimide; isobutyl chloroformate; In diethyl ether; chloroform; acetone;

Reference yield:

: 79821-93-5
HCl, H-Lys(Z)-Leu-ONp

: 123795-48-2
(S)-2-((S)-6-Benzyloxycarbonylamino-2-{(S)-6-benzyloxycarbonylamino-2-[(S)-4-methyl-2-(2-nitro-phenylsulfanylamino)-pentanoylamino]-hexanoylamino}-hexanoylamino)-4-methyl-pentanoic acid 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / DCC / CHCl₃ / 1. -10 deg C, 2 h; 2. room temperature, 2 h

2: 91 percent / HCl / acetone; diethyl ether / 0.25 h

3: 1. N-methylmorpholine, isobutyl chloroformate; 2. N-methylmorpholine / 1. THF, -10 deg C, 15 min; 2. -10 deg C, 1 h, room temperature, 2 h

With 4-methyl-morpholine; hydrogenchloride; dicyclohexyl-carbodiimide; isobutyl chloroformate; In diethyl ether; chloroform; acetone;

Reference yield:

: 123795-46-0
(S)-2-{(S)-6-Benzyloxycarbonylamino-2-[(S)-6-benzyloxycarbonylamino-2-(2-nitro-phenylsulfanylamino)-hexanoylamino]-hexanoylamino}-4-methyl-pentanoic acid 4-nitro-phenyl ester

: 123795-48-2
(S)-2-((S)-6-Benzyloxycarbonylamino-2-{(S)-6-benzyloxycarbonylamino-2-[(S)-4-methyl-2-(2-nitro-phenylsulfanylamino)-pentanoylamino]-hexanoylamino}-hexanoylamino)-4-methyl-pentanoic acid 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / HCl / acetone; diethyl ether / 0.25 h

2: 1. N-methylmorpholine, isobutyl chloroformate; 2. N-methylmorpholine / 1. THF, -10 deg C, 15 min; 2. -10 deg C, 1 h, room temperature, 2 h

With 4-methyl-morpholine; hydrogenchloride; isobutyl chloroformate; In diethyl ether; acetone;