3S-benzoyloxy-2R-benzoyloxymethyl-5S-(2-phenylthiazol-4-yl)-tetrahydrofuran

Base Information

Chemical Name:3S-benzoyloxy-2R-benzoyloxymethyl-5S-(2-phenylthiazol-4-yl)-tetrahydrofuran
CAS No.:675124-57-9
Molecular Formula:C₂₈H₂₃NO₅S
Molecular Weight:485.56
Hs Code.:

Synonyms:3S-benzoyloxy-2R-benzoyloxymethyl-5S-(2-phenylthiazol-4-yl)-tetrahydrofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3S-benzoyloxy-2R-benzoyloxymethyl-5S-(2-phenylthiazol-4-yl)-tetrahydrofuran

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Technology Process of 3S-benzoyloxy-2R-benzoyloxymethyl-5S-(2-phenylthiazol-4-yl)-tetrahydrofuran

There total 4 articles about 3S-benzoyloxy-2R-benzoyloxymethyl-5S-(2-phenylthiazol-4-yl)-tetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 2227-79-4
benzenecarbothioamide

: 675124-53-5
2-chloro-1-(4S-benzoyloxy-5R-benzoyloxymethyl-tetrahydrofuran-2R/S-yl)-ethanone

: 675124-56-8
3S-benzoyloxy-2R-benzoyloxymethyl-5R-(2-phenylthiazol-4-yl)-tetrahydrofuran

: 675124-57-9
3S-benzoyloxy-2R-benzoyloxymethyl-5S-(2-phenylthiazol-4-yl)-tetrahydrofuran

Guidance literature:: In ethanol; for 20h; Heating;
DOI:10.1016/j.tet.2003.11.055

Reference yield:

: 108647-88-7
((2R,3S)-3-(benzoyloxy)-5-methoxytetrahydrofuran-2-yl)methyl benzoate

: 675124-57-9
3S-benzoyloxy-2R-benzoyloxymethyl-5S-(2-phenylthiazol-4-yl)-tetrahydrofuran

Guidance literature:: Multi-step reaction with 5 steps

1.1: 71 percent / BF₃*OEt₂ / CH₂Cl₂ / 1.5 h / 0 °C

2.1: 72 percent / hydrochloric acid / dioxane / 6 h / 80 °C

3.1: α,α-dichloromethyl methyl ether / CH2Cl2 / 4 h / Heating

4.1: diethyl ether / 0.25 h

4.2: 61 percent / HCl gas / diethyl ether / 0.5 h

5.1: 22 percent / ethanol / 20 h / Heating

With hydrogenchloride; Dichloromethyl methyl ether; boron trifluoride diethyl etherate; In 1,4-dioxane; diethyl ether; ethanol; dichloromethane;
DOI:10.1016/j.tet.2003.11.055

Reference yield:

: 675124-51-3
2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-D-arabino- and D-ribo-hexonic acid

: 675124-57-9
3S-benzoyloxy-2R-benzoyloxymethyl-5S-(2-phenylthiazol-4-yl)-tetrahydrofuran

Guidance literature:: Multi-step reaction with 3 steps

1.1: α,α-dichloromethyl methyl ether / CH2Cl2 / 4 h / Heating

2.1: diethyl ether / 0.25 h

2.2: 61 percent / HCl gas / diethyl ether / 0.5 h

3.1: 22 percent / ethanol / 20 h / Heating

With Dichloromethyl methyl ether; In diethyl ether; ethanol; dichloromethane;
DOI:10.1016/j.tet.2003.11.055