N-{9-[4-hydroxy-3-methoxy-5-([2,2';6',2'']terpyridin-4'-yloxymethyl)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide

Base Information

Chemical Name:N-{9-[4-hydroxy-3-methoxy-5-([2,2';6',2'']terpyridin-4'-yloxymethyl)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide
CAS No.:222171-14-4
Molecular Formula:C₃₃H₂₈N₈O₅
Molecular Weight:616.636
Hs Code.:

<i>N</i>-{9-[4-hydroxy-3-methoxy-5-([2,2';6',2'']terpyridin-4'-yloxymethyl)-tetrahydro-furan-2-yl]-9<i>H</i>-purin-6-yl}-benzamide

Synonyms:N-{9-[4-hydroxy-3-methoxy-5-([2,2';6',2'']terpyridin-4'-yloxymethyl)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide

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Chemical Property of N-{9-[4-hydroxy-3-methoxy-5-([2,2';6',2'']terpyridin-4'-yloxymethyl)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide

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Technology Process of N-{9-[4-hydroxy-3-methoxy-5-([2,2';6',2'']terpyridin-4'-yloxymethyl)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide

There total 9 articles about N-{9-[4-hydroxy-3-methoxy-5-([2,2';6',2'']terpyridin-4'-yloxymethyl)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 128143-89-5
4'-Chloro-2,2':6',2''-terpyridine

: 222171-14-4
N-{9-[4-hydroxy-3-methoxy-5-([2,2';6',2'']terpyridin-4'-yloxymethyl)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / KOH / dimethylsulfoxide / 44 h

2: 100 percent / MeCOOH, H₂O / 4 h

3: pyridine / 0.5 h

4: 3.5 h

5: 1.) H₂O, 2.) NH₄OH, H₂O / 1.) 5 min, 2.) 30 min

With pyridine; potassium hydroxide; ammonium hydroxide; water; acetic acid; In dimethyl sulfoxide;
DOI:10.1039/a808522f

Reference yield:

: 2140-79-6
2'-O-methyl adenosine

: 222171-14-4
N-{9-[4-hydroxy-3-methoxy-5-([2,2';6',2'']terpyridin-4'-yloxymethyl)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide

Guidance literature:: Multi-step reaction with 8 steps

1: 77 percent / imidazole / dimethylformamide / 1.5 h

2: 77 percent / pyridine / 23 h

3: 99 percent / Bu₄NF / tetrahydrofuran / 0.5 h

4: 90 percent / KOH / dimethylsulfoxide / 44 h

5: 100 percent / MeCOOH, H₂O / 4 h

6: pyridine / 0.5 h

7: 3.5 h

8: 1.) H₂O, 2.) NH₄OH, H₂O / 1.) 5 min, 2.) 30 min

With pyridine; 1H-imidazole; potassium hydroxide; ammonium hydroxide; tetrabutyl ammonium fluoride; water; acetic acid; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1039/a808522f

Reference yield:

: 221537-14-0
2'-methyl-adenosine

: 222171-14-4
N-{9-[4-hydroxy-3-methoxy-5-([2,2';6',2'']terpyridin-4'-yloxymethyl)-tetrahydro-furan-2-yl]-9H-purin-6-yl}-benzamide

Guidance literature:: Multi-step reaction with 7 steps

1: 77 percent / pyridine / 23 h

2: 99 percent / Bu₄NF / tetrahydrofuran / 0.5 h

3: 90 percent / KOH / dimethylsulfoxide / 44 h

4: 100 percent / MeCOOH, H₂O / 4 h

5: pyridine / 0.5 h

6: 3.5 h

7: 1.) H₂O, 2.) NH₄OH, H₂O / 1.) 5 min, 2.) 30 min

With pyridine; potassium hydroxide; ammonium hydroxide; tetrabutyl ammonium fluoride; water; acetic acid; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1039/a808522f