N-{6-[3-(N-cholesteryl-2-nitrobenzenesulfonamido)propylamino]-6-oxohexyl}biotinamide

Base Information

Chemical Name:N-{6-[3-(N-cholesteryl-2-nitrobenzenesulfonamido)propylamino]-6-oxohexyl}biotinamide
CAS No.:440358-98-5
Molecular Formula:C₅₂H₈₂N₆O₇S₂
Molecular Weight:967.391
Hs Code.:

Synonyms:N-{6-[3-(N-cholesteryl-2-nitrobenzenesulfonamido)propylamino]-6-oxohexyl}biotinamide

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Chemical Property of N-{6-[3-(N-cholesteryl-2-nitrobenzenesulfonamido)propylamino]-6-oxohexyl}biotinamide

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Technology Process of N-{6-[3-(N-cholesteryl-2-nitrobenzenesulfonamido)propylamino]-6-oxohexyl}biotinamide

There total 3 articles about N-{6-[3-(N-cholesteryl-2-nitrobenzenesulfonamido)propylamino]-6-oxohexyl}biotinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89889-52-1
biotinamidocaproate N-hydroxysuccinimide ester

: N-(3-Amino-propyl)-N-[(3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl]-2-nitro-benzenesulfonamide

: 440358-98-5
N-{6-[3-(N-cholesteryl-2-nitrobenzenesulfonamido)propylamino]-6-oxohexyl}biotinamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 25 ℃; for 2h;
DOI:10.1021/ja0258733

Reference yield:

: 390762-93-3
N-cholesteryl-2-nitrobenzenesulfonamide

: 440358-98-5
N-{6-[3-(N-cholesteryl-2-nitrobenzenesulfonamido)propylamino]-6-oxohexyl}biotinamide

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / potassium carbonate / N,N-dimethyl-acetamide / 12 h / 120 °C

2: trifluoroacetic acid / CH₂Cl₂ / 0.75 h / 25 °C

3: 49 mg / diisopropylethylamine / CH₂Cl₂ / 2 h / 25 °C

With potassium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl acetamide;
DOI:10.1021/ja0258733

Reference yield:

: 440358-97-4
N-[3-(tert-butoxycarbonylamino)propyl]-N-cholesteryl-2-nitrobenzenesulfonamide

: 440358-98-5
N-{6-[3-(N-cholesteryl-2-nitrobenzenesulfonamido)propylamino]-6-oxohexyl}biotinamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / CH₂Cl₂ / 0.75 h / 25 °C

2: 49 mg / diisopropylethylamine / CH₂Cl₂ / 2 h / 25 °C

With N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/ja0258733