(Z)-2-(1-(3-methylphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(Z)-2-(1-(3-methylphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1402235-26-0
Molecular Formula:C₁₆H₂₃BO₂
Molecular Weight:258.168
Hs Code.:

Synonyms:(Z)-2-(1-(3-methylphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of (Z)-2-(1-(3-methylphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of (Z)-2-(1-(3-methylphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 3 articles about (Z)-2-(1-(3-methylphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1402235-30-6
2-(3-(3-methylphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1402235-26-0
(Z)-2-(1-(3-methylphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With C₂₇H₄₀Cl₂FeN₃P; sodium triethylborohydride; In pentane; at 20 ℃; for 8h; stereoselective reaction;
DOI:10.1021/acscatal.1c02432

Reference yield: 70.0%

: 29816-85-1
1-methyl-3-(propa-1,2-dien-1-yl)benzene

: 73183-34-3
bis(pinacol)diborane

: 1402235-26-0
(Z)-2-(1-(3-methylphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With methanol; P(p-CH₃OC₆H₄)3; copper(l) chloride; sodium t-butanolate; In diethyl ether; at 20 ℃; for 0.833333h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201100929

Reference yield:

: 18826-62-5
1-methyl-3-(prop-1-yn-1-yl)benzene

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1402235-26-0
(Z)-2-(1-(3-methylphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: (Z)-4,4,5,5-tetramethyl-2-(1-(m-tolyl)prop-1-en-1-yl)-1,3,2-dioxaborolane

Guidance literature:: 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; With 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; cobalt acetylacetonate; In tetrahydrofuran; at 20 ℃; for 0.25h; Inert atmosphere; Schlenk technique;

1-methyl-3-(prop-1-yn-1-yl)benzene; In tetrahydrofuran; at 20 ℃; for 16h; Overall yield = 83 percent; Overall yield = 85.48 mg; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.1c02854