3,10-dibromo-5,7,12,14-tetrahydro-5,5,12,12-tetra(p-octylphenyl)-7,7,14,14-tetraphenyl-di(indeno[2,1-a:2’,1’-d’])-s-indacene

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Chemical Name:3,10-dibromo-5,7,12,14-tetrahydro-5,5,12,12-tetra(p-octylphenyl)-7,7,14,14-tetraphenyl-di(indeno[2,1-a:2’,1’-d’])-s-indacene
CAS No.:1334701-49-3
Molecular Formula:C₁₀₆H₁₁₂Br₂
Molecular Weight:1545.86
Hs Code.:

Synonyms:3,10-dibromo-5,7,12,14-tetrahydro-5,5,12,12-tetra(p-octylphenyl)-7,7,14,14-tetraphenyl-di(indeno[2,1-a:2’,1’-d’])-s-indacene

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Chemical Property of 3,10-dibromo-5,7,12,14-tetrahydro-5,5,12,12-tetra(p-octylphenyl)-7,7,14,14-tetraphenyl-di(indeno[2,1-a:2’,1’-d’])-s-indacene

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Technology Process of 3,10-dibromo-5,7,12,14-tetrahydro-5,5,12,12-tetra(p-octylphenyl)-7,7,14,14-tetraphenyl-di(indeno[2,1-a:2’,1’-d’])-s-indacene

There total 1 articles about 3,10-dibromo-5,7,12,14-tetrahydro-5,5,12,12-tetra(p-octylphenyl)-7,7,14,14-tetraphenyl-di(indeno[2,1-a:2’,1’-d’])-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1334701-43-7
5,7,12,14-tetrahydro-5,5,12,12-tetra(p-octylphenyl)-7,7,14,14-tetraphenyl-di(indeno[2,1-a:2’,1’-d’])-s-indacene

: 1334701-49-3
3,10-dibromo-5,7,12,14-tetrahydro-5,5,12,12-tetra(p-octylphenyl)-7,7,14,14-tetraphenyl-di(indeno[2,1-a:2’,1’-d’])-s-indacene

Guidance literature:: With aluminum oxide; copper(ll) bromide; In tetrachloromethane; at 85 ℃; for 12h;
DOI:10.1021/ja206060n

Reference yield: 97.0%

: 1334701-49-3
3,10-dibromo-5,7,12,14-tetrahydro-5,5,12,12-tetra(p-octylphenyl)-7,7,14,14-tetraphenyl-di(indeno[2,1-a:2’,1’-d’])-s-indacene

: 1334701-44-8
3,10-diiodo-5,7,12,14-tetrahydro-5,5,12,12-tetra(p-octylphenyl)-7,7,14,14-tetraphenyl-di(indeno[2,1-a:2’,1’-d’])-s-indacene

Guidance literature:: 3,10-dibromo-5,7,12,14-tetrahydro-5,5,12,12-tetra(p-octylphenyl)-7,7,14,14-tetraphenyl-di(indeno[2,1-a:2’,1’-d’])-s-indacene; With n-butyllithium; In diethyl ether; hexane; at 0 ℃; for 1h; Inert atmosphere;

With 1,2-Diiodoethane; In diethyl ether; hexane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja206060n

Reference yield: 95.0%

: 1334701-49-3
3,10-dibromo-5,7,12,14-tetrahydro-5,5,12,12-tetra(p-octylphenyl)-7,7,14,14-tetraphenyl-di(indeno[2,1-a:2’,1’-d’])-s-indacene

: 122-39-4
diphenylamine

: C₁₃₀H₁₃₂N₂

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; In toluene; at 110 ℃; Inert atmosphere;
DOI:10.1021/ja5125463