2-(Bis-{[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethylcarbamoyl]-methyl}-amino)-N-[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethyl]-acetamide

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Chemical Name:2-(Bis-{[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethylcarbamoyl]-methyl}-amino)-N-[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethyl]-acetamide
CAS No.:191109-56-5
Molecular Formula:C₃₃H₄₂N₄O₉
Molecular Weight:638.718
Hs Code.:

Synonyms:2-(Bis-{[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethylcarbamoyl]-methyl}-amino)-N-[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethyl]-acetamide

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Chemical Property of 2-(Bis-{[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethylcarbamoyl]-methyl}-amino)-N-[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethyl]-acetamide

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Technology Process of 2-(Bis-{[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethylcarbamoyl]-methyl}-amino)-N-[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethyl]-acetamide

There total 4 articles about 2-(Bis-{[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethylcarbamoyl]-methyl}-amino)-N-[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 22241-07-2
nitrilotriacetic acid trimethyl ester

: 191109-48-5
(S)-2-amino-2-(4-methoxyphenyl)-1-ethanol

: 191109-56-5
2-(Bis-{[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethylcarbamoyl]-methyl}-amino)-N-[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethyl]-acetamide

Guidance literature:: at 80 ℃; for 40h;
DOI:10.1016/S0040-4020(97)00322-0

Reference yield:

: 13603-63-9,147159-72-6,147254-29-3,32345-64-5
(R)-1-(4-methoxyphenyl)ethane-1,2-diol

: 191109-56-5
2-(Bis-{[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethylcarbamoyl]-methyl}-amino)-N-[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethyl]-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: NaOH

2: NaN₃, H₂O / dimethylformamide

3: 56 percent / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

4: 74 percent / 40 h / 80 °C

With sodium hydroxide; lithium aluminium tetrahydride; sodium azide; water; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)00322-0

Reference yield:

: 191109-43-0
(R)-4-(p-methoxyphenyl)-1,3-dioxolane-2-one

: 191109-56-5
2-(Bis-{[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethylcarbamoyl]-methyl}-amino)-N-[(S)-2-hydroxy-1-(4-methoxy-phenyl)-ethyl]-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: NaN₃, H₂O / dimethylformamide

2: 56 percent / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

3: 74 percent / 40 h / 80 °C

With lithium aluminium tetrahydride; sodium azide; water; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)00322-0