3-methyl-1-[2-(1-piperidinyl)phenyl]butoxime

Base Information Edit

Chemical Name:3-methyl-1-[2-(1-piperidinyl)phenyl]butoxime
CAS No.:765306-65-8
Molecular Formula:C₁₆H₂₄N₂O
Molecular Weight:260.379
Hs Code.:
Mol file:765306-65-8.mol

Synonyms:3-methyl-1-[2-(1-piperidinyl)phenyl]butoxime

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Chemical Property of 3-methyl-1-[2-(1-piperidinyl)phenyl]butoxime Edit

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Technology Process of 3-methyl-1-[2-(1-piperidinyl)phenyl]butoxime

There total 4 articles about 3-methyl-1-[2-(1-piperidinyl)phenyl]butoxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 147770-03-4
3-methyl-1-(2-piperidin-1-yl-phenyl)-butan-1-one

: 765306-65-8
3-methyl-1-[2-(1-piperidinyl)phenyl]butoxime

Guidance literature:: With sodium hydroxide; hydroxylamine hydrochloride; In ethanol; at 20 ℃; for 3h;

Reference yield:

: 446-52-6
2-Fluorobenzaldehyde

: 765306-65-8
3-methyl-1-[2-(1-piperidinyl)phenyl]butoxime

Guidance literature:: Multi-step reaction with 4 steps

1.1: magnesium; iodine / tetrahydrofuran; toluene / 4 h / 20 - 40 °C / Inert atmosphere

1.2: 6 h / 10 °C / Inert atmosphere

2.1: sulfuric acid; sodium hypochlorite / dichloromethane / 15 - 20 °C

3.1: 3 h / Reflux

4.1: hydroxylamine hydrochloride; sodium hydroxide / 20 - 25 °C

With sodium hypochlorite; sulfuric acid; hydroxylamine hydrochloride; iodine; magnesium; sodium hydroxide; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 147769-96-8
3-methyl-1-[2-(piperidin-1-yl)phenyl]butan-1-imine

: 765306-65-8
3-methyl-1-[2-(1-piperidinyl)phenyl]butoxime

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; water / 0.67 h / 20 °C

2: hydroxylamine hydrochloride; sodium hydroxide / 20 - 25 °C

With sulfuric acid; hydroxylamine hydrochloride; water; sodium hydroxide;