N-(3-aminopropyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide fumarate

Base Information

Chemical Name:N-(3-aminopropyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide fumarate
CAS No.:1350977-94-4
Molecular Formula:C₄H₄O₄*C₂₁H₂₉N₃O₂S
Molecular Weight:503.62
Hs Code.:

Synonyms:N-(3-aminopropyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide fumarate

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Chemical Property of N-(3-aminopropyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide fumarate

Chemical Property:

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Technology Process of N-(3-aminopropyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide fumarate

There total 5 articles about N-(3-aminopropyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide fumarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350977-93-3
N-(3-aminopropyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide

: 110-17-8,26099-09-2
(2E)-but-2-enedioic acid

: 1350977-94-4
N-(3-aminopropyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide fumarate

Guidance literature:: In acetone; at 20 ℃;
DOI:10.1016/j.bmc.2011.09.044

Reference yield:

: N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide

: 1350977-94-4
N-(3-aminopropyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide fumarate

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutylammomium bromide; potassium carbonate; sodium hydroxide / toluene / 18 h / 60 °C / Reflux

2.1: hydrazine / ethanol / 1 h / Reflux

2.2: 4 h / Reflux

3.1: acetone / 20 °C

With tetrabutylammomium bromide; potassium carbonate; sodium hydroxide; hydrazine; In ethanol; acetone; toluene;
DOI:10.1016/j.bmc.2011.09.044

Reference yield:

: 5596-87-2
3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propan-1-amine

: 1350977-94-4
N-(3-aminopropyl)-N-[3-(1,2,3,4-tetrahydroisoquinolin-2-yl)propyl]benzenesulfonamide fumarate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / water / 0.5 h / 60 °C

2.1: tetrabutylammomium bromide; potassium carbonate; sodium hydroxide / toluene / 18 h / 60 °C / Reflux

3.1: hydrazine / ethanol / 1 h / Reflux

3.2: 4 h / Reflux

4.1: acetone / 20 °C

With tetrabutylammomium bromide; potassium carbonate; sodium hydroxide; hydrazine; In ethanol; water; acetone; toluene;
DOI:10.1016/j.bmc.2011.09.044